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GCMS analysis results for sample AE10813, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry report for sample AE10813 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000046064–000046080

Folder label: “GCMS X 5/7/02 A 5/15/02

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NYC 9/11 Public Portal Document

‘Data File : C:\MSDCHEM\1\DATA\051402\10813.D Vial 23 Acq On : 15 May 2002 8:17 am Operator Mclean Sample : 5/7 kb Inst Instrumen Mise Multiplr 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 N-Acetyltranylcypromine Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

34.90 0.40 ug/L 284838 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Acetyltranylcypromine 175 C11H13NO 078682-61-8 9 2 Benzene, 1-chloro -4 -fluoro- 130 C6H4C1F 000352-33-0 9 3 Ethane, 1,2 -Bis(1-phenylcyclopro... 262 C20H22 1000210-95-2 9 4 3-Ethylthiolane 116 C6H12S 1000215-08-2 5 Abundance Scan 5416 (34.901 min): 10813.D (-5414) (-) m/z 130.10 100.00% 130

118 44 73 281 5000 209 1 1 । . ' . . । 265 34.60 34.80 35.00 35.20 1 1 - . ------------------------------------- m/z 117.90 62.03% OTT m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #59666: N-Acetyltranylcypromine 132 116 T I [ 4 I I [ i 7- T ] ) I I I [ I I I । |

5000 60 84 34.60 34.80 35.00 35.20 103 m/z 132.05 57.22%

m/z-> 20 ....... I, 0- 1 i ' ' ■ ' i 1 ' 1 40 60 ' 1 ' i 80 LL ll.r T 146 | ii'i

100 120 140 160 180 200 220 r i I 175 II | 1 I I I | 1 T • । ■1 1 11111 ■ ।'1111'1 240 260 280 Abundance #58738: Benzene, 1-chloro-4-fluoro- 110

34.60 34.80 35.00 35.20 5000 95 m/z 73.20 54.43% 73

25 37 50 4 1 1 1 ' 1 TTTTT o1 I I I I r I I I I I , I , 109 I I I ' i 1 1 1 1 i 1 1 1 ' i 1 1 1 1 i ' 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #58809: Ethane, 1,2-Bis(1-phenylcyclopropyl)- 11 7130 34.60 34.80 35.00 35.20 91 m/z 44.10 53.42%

5000 103 143 mWWlw/yjywhMeyhapyp v 77 27 39 51 65 158 0 1,7.44 lTTTT I T d—— T-n .I 171 193.205 I, TTTTT T——OC—nTT 220233 247 262 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20

10813 .D 050102.M Thu May 16 14:15:52 2002 Page 11

NYC-WTC_000046079

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NYC-WTC_000046079Source: NYC Law Department, mirrored locally

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