GCMS analysis results, Sample AE08267, April 22, 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08267.D Vial: 24 Acq On 18 Apr 2002 4:22 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 N-Acetyltranylcypromine Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

35.03 0.28 ug/L 319616 Perylene-dl2 34.79

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 N-Acetyltranylcypromine 175 C11H13NO 078682-61-8 9 2 Benzenemethanol, 2,4,5-trimethyl- 150 C1OH140 004393-05-9 9 3 Trichloroethylene 130 C2HC13 000079-01-6 5 4 1,3-Cyclopentanedione, 2-chloro- 132 C5H5C1O2 014203-19-1 5 Abundance Scan 5437 (35.025 m;n). 08267.D (-5435) (-) m/z 40.00 100.00% 43

132

5000 73 207 118 281 262 34 60 34 80 35 00 35 20 35 40 — 0+1 i 1 1 m/z 132.10 66.83% n/z- > 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #59666' N-Acetyltranylcypromine 13 2

116

5000 60 84 34.60 34.80 35.00 35.20 35.40 105 m/z 129.80 48.50%

n/z-> 20 0 l ■ ■ ■ 1 I 1 ■ 40 60 1 *। 80 LL 100 || 120 146 140 160 175 180 200 220 240 260 280 Abundance #59790: Benzenemethanol, 2,4,5-trimethy- 12 2

150 91 107 34.60 34.80 35.00 35.20 35.40 5000 m/z73.00 32.83% 77 119

Tl/Z—> 0+IIT 20 40 60 AAdal 80 100 120 140 160 + 180 200 220 240 260 280 h M Abundance 95 #121902 Trichloroethylene 130 144 4 34 60 34 80 35 00 35 20 35 40 m/z 207.00 31.33% 5000

Tl/Z— > 0 20 + 35 47 40 60

11.72.33, I, 112,, 60 80 100 120 140 160 180 200 220 240 260 280 J yuMMrn 34.60 34.80 35.00 35.20 35.40

08267 .D 041702SCAN.M Thu Apr 18 10:01:03 2002 Page 10

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