GCMS analysis results, Sample AE08267, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08267.D Vial: 24 Acq On : 18 Apr 2002 4:22 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Acetonitrile, bromo- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.02 0.31 ug/L 467166 Chrysene-dl2 30.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, bromo- 119 C2H2BrN 000590-17-0 5 24-(Pentafluoropropanamido)pyridine 240 C8H5F5N2O 1000104-00-4 5 3 Carbamothioic acid, 0-isopropyl .. 119 C4H9NOS 000691-61-2 4 4 Benzene, (1,1-dimethylnonyl)- 232 C17H28 055191-25-8 4 Abundance Scan 4756 (31 023 min) 08267.D (-4755) (-) m/z 40.00 100.00% 4) 240

119 5000 78 102 208

30 60 30 80 31.00 31.20 31.40 0+ T11/1 i r i p m/z 240.20 82.54% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #108421: Acetonitrile, bromo- 43 119

5000 114, — ■ । । 1 ■ 30.60 30.80 31 00 31 20 31.40 79 m/z 119.20 54.96% 92 0+ 14 । 28, 11. TIr n/z- > Abundance 20 40 60 80 100 120 140 160 180 200 220 240 #91285: 4-(Pentaf!uoropropanamido)pyridine 240

78 ‘‘‘I’’’ "II M 30.60 30.80 31 00 31 20 31.40 121 5000 m/z 44.00 36.31%

51 — WWMsMWWHinpp 01 n/z— > 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #53111 Carbamothioic acid, O-isopropyl ester 44 1 9 30.60 30.80 31.00 31.20 31.40 77 m/z 208.10 34.92% 5000 27 60

n/z—> 0 P20 40 il 60 lli 80 100 ------------- 120 140 160 180 200 220 240 30.60 30.80 31 00 31 20 31.40

08267.D 041702SCAN.M Thu Apr 18 10:01:03 2002 Page 9

NYC-WTC_000048433