GCMS analysis results, sample AE07514, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07514.D Vial: 10 Acq On 4 Apr 2002 3:22 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Acetic acid, 2-propenyl ester Concentration Rank 1

R.T. EstConc Area Relative to ISTD- R.T.

5.59 0.26 ug/1 194547 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 2-propenyl ester 100 C5H802 000591-87-7 2 2 Acetamide, N-(3-methyl-2-oxobutyl)- 143 C7H13N02 082479-25-2 2 3 3-Pentyn-2-one, 5,5-diethoxy- 170 C9H14O3 055402-04-5 2 4 2-Butanol, 2-nitroso-, acetate (... 145 C6H11NO3 013880-90-5 2 Abundance Scan 427 (5.588 min): 07514.D (-421) (-) m/ z 43.10 100.00% 43

5000

I,............. 73 84 125 5.20 5.40 m 5.60 5.80 6.00 Of ' I ' ''' I' ' ’ I' TTII’’’ 1 {' 11111111 I''' ' I'1'' I' ‘' 1 1'' 11' '1' I ■ i > • > ■ i ■1 • ■ i ■ ■ m/z 73.10 23.16% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #109540: Acetic acid, 2-propenyl ester 43

5000 56 5.20 5.40 5.60 5.80 6.00 73 m/z 124.90 12.02% 85 ’100OtuTTT n/z-> 01 1 I ' ' ' ' I ' 20 30 1 * rurpi r TTP’Iu i ■ ■ ■ ■ i i1 ■ ■ ■ i ‘ • i'' 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #4003: Acetamide, N-(3-methyl-2-oxobutyl)- 30 43

5.20 5.40 5.60 5.80 6.00 5000 m/ Z 47.10 11.33% 72 100

1 60 I 86 O+ - I +-HH—— ""I1-1 110 128 144 ■ ■ i ■ ■ ■ ■ । > > > ■ 11 ■ ■ ■ i ■ । ■ 11 • ■ ■ । ■ i ■ ■ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #5306: 3-Pentyn-2-one, 5,5-diethoxy- 43 5.20 5.40 5.60 5.80 6.00 m/z 84.00 5.05% 5000 55

83 97 "MMAWMwpy 125 ! 69 ...I 0 '11 ''1I''''I' ... - ... 1 1.... 1 , 141 169 '11'11i' 1 1 r i'' 1 ' r ' ‘11' ' n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 5.20 5.40 5.60 5.80 6.00

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