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GCMS analysis results, sample AE07510, April 2002

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Laboratory report documenting GCMS analysis of environmental sample AE07510 conducted on April 11, 2002.

NYC-WTC_000047322–000047332

Folder label: “GCMS X 4/2/02 A 4/4/02

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Scanned page image, NYC-WTC_000047330
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020404\07510.D Vial: 6 Acq On 4 Apr 2002 11:39 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1\METHODS\SCAN020403 . M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 Acetic acid, 2-propenyl ester Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.59 0.18 ug/1 128308 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 2-propenyl ester 100 C5H802 000591-87-7 2 2 1-Butanamine 73 C4H11N 000109-73-9 1 3 N-Ethylformamide 73 C3H7NO 000627-45-2 1 4 1-Propanamine, 2-methyl- 73 C4H11N 000078-81-9 1 Abundance Scan 427 (5.588 min): 07510.D (-419) (-) m/ z 43.10 100.00% 43

5000 73 — ■ I ■ ■ 1 ■ I ■ 125 5.20 5.40 5.60 580 6.00 0 * 49___________ ''l ' ' ' ' I ' ‘ ' ' I 1 ' ' ' I ' 84........................ | 1 m/ z 73.10 26.56% m/z-> 10 20 30 40 50 60 70 80i 90 100 110 120 130 Abundance #109540: Acetic acid, 2-propenyl ester 43

5000 56 5.20 5.40 5.60 5.80 6.00 73 m/z 124.90 11.52% 49 85 100 01 — TPPT n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #108242:1-Butanamine 33

5.20 5.40 5.60 5.80 6.00 5000 m/z 40.10 5.32%

73 41 50 56 65 _L_ 01 ----- -+ "dt 1TTU, ' i ■ ■ ' ■ i ■ ' 1 ' i ■ ' ' 1 i 1 ■ ■ ' i ' ■ ■ ■ i ' 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #&5T: N-Ethylformamide 33 5.20 5.40 5.60 5.80 6.00 73 m/z 49.00 2.43% 5000 44 58 18 0 —P10, 1. 3811 . । ■ ■i' ■1' i'1 ■ ■ । ■' ■ ■ । ■1 ■11'111111'111111 r11 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 5.20 5.40 5.60 5.80 6.00

NYC-WTC_000047330

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NYC-WTC_000047330Source: NYC Law Department, mirrored locally

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