GCMS analysis results for sample AE07631, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020403\07630FB.D Vial: 15 Acq On 3 Apr 2002 10:00 pm Operator: Nefliu Sample 07630 field blk Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 1-Propanamine, 2-methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.57 0.13 ug/1 97260 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propanamine, 2-methyl- 73 C4H11N 000078-81-9 2 2 Guanidine, methyl- 73 C2H7N3 000471-29-4 2 3 N-Ethylformamide 73 C3H7NO 000627-45-2 2 4 1-Propanamine, 2-methyl- 73 C4H11N 000078-81-9 1 Abundance Scan 424 (5.570 min): 07630FB.D (-418) (-) m/ z 73.10 100.00% 73

5000 \ 40 43 1 1 1 ' 1 1 I ' ' ' I ' 1 1 ' I 1 1 1 1 1 1 520 5.40 560 5.80 6.00 Ot ' i " '' i'1 " i " " i'1 ■' i ■ ■ ■ ■ i'' 111'111" m/z 43.10 31.85% n/z-> 5 10 15 20 25 3035 40 45 50 55 60 65 70 75 80 Abundance #677:1-Propanamine, 2-methyl- 30

5000 5.20 5.40 5.60 5.80 6.00 m/z 40.10 31.80% 12 1,5 18 27, ,1133■ ■ । 38 41 44 49 52 56 59 70 73 Of I ■ ■•i • ■ ■ ■ 111111 > > > >।> 11+ ■ n 111111 ■ ■ ■ ■ । ■ 11111 ■ [. ■ ■ ■ । ■ ■ ■ ■ । ■1111 > > ।1111 n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #759: Guanidine, methyl- 30 43 73 5.20 5.40 5.60 5.80 6.00 5000 18

57

n/z-> 01 5 10 15

15 -++ 20 25 27 30 11111 1111 35 40 .... 45 50 55 - 60 65 70 11'1 ■' i'1

75 80 Abundance #857: N-Ethylformamide 30 73

5000 44 58 27 15 18 m/z-> 0 I I I 1 I I I I I 1 I I I I H+ — 1 —H 5 10 15 20 25 1TTTT 38411444 54 ' 111 1 I | i r i > । I if i" । I > 11 ■' ■1111 30 35 40 45 50 55 60 65 70 75 80

07630FB.D SCAN020403.M Thu Apr 04 10:48:40 2002 Page 4

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