GCMS analysis results for sample AE07631, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020403\07630FB.D Vial: 15 Acq On 3 Apr 2002 10:00 pm Operator: Nefliu Sample 07630 field blk Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 Heptasiloxane, 1,1,3,3,5,5,. Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 14.69 0.22 ug/1 218381 Naphthalene-d8 15.77

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9 9 2 6H-Dibenzo[a,g]quinolizine, 5,8,... 355 C21H25NO4 002934-97-6 5 3 Cobalt, bis(.eta.-5-piperidinylc... 355 C20H28CON2 1000162-04-6 5 4 7H-Dibenzo[c ,g]carbazole 267 C20H13N 000194-59-2 5 Abundance Scan 1976 (14.689 min): 07630FB.D (-1967) (-) m/ z 73.10 100.00% 73

267 355 5000

40 14.40 14.60 14.80 15.00 0- 1’’ m/z 355.00 52.50% m/z—> 50 100 150 200 250 300 350 400 450 Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tet... 73

5000 207 14.40 14.60 14.80 15.00 m/z 267.00 50.96% 133 2811 355 0- , 45 I 1 ‘1 1 103, 177 1 / . Il— *d**** TTTm.n 2531 l 327, I 377399 429 489 n/z-> 50 100 150 200 250300 350 400 450 Abundance #128845: 6H-Dibenzo[a,g]quinolizine, 5,8,13,13a-tetrahydro... 355 149 14.40 14.60 14.80 15.00 5000 m/z 40.10 18.02% 190 324 77 121 0- 44 TH Pit 4+4220 264 294. ■i T i-1 t”| + f n/z-> 50 100 150 200 250 300 350 400 450 Abundance #103471: Cobalt, bis(.eta.-5-piperidinylcyclopentadienyl)- 1 I I ■ I I I I I 1 I I I I ' I I I I I I 355 14.40 14.60 14.80 15.00 m/z 356.00 17.45% } 5000

31 59 92 124148 178 202 242 272 299 325 0 ’ i '■ ’ ■ 1 ■ i 1 ■■ ■ 1 'i'' r ■ 1 /1 ■ FI’ r 1 1 i 1 1 ‘1 1 r1 । । । । 1 1 1 1 । 1 n/z-> 50 100 150 200 250 300 350 400 450 14.40 14.60 14.80 15.00

07630FB.D SCAN020403.M Thu Apr 04 10:48:42 2002 Page 5

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