NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\020410\0403LB.D Vial: 3
Acq On : 10 Apr 2002 12:20 pm Operator: Nefliu
Sample : 04/03 lab blk Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1. .. \SCANAPR0902.M (Chemstation Integrator)
Title : Method 508 GC/MS Scan
Library : C:\DATABASE\nist98.1
*********************************************************************
Peak Number 1 Heptasiloxane, 1,1,3,3,5,5,. Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.68 0.33 ug/1 270199 Naphthalene-d8 15.76
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9 9
2 Codein-propionyl 355 C21H25NO4 065644-90-8 5
3 1,3-Benzodioxole-5-ethanamine , 6... 355 C21H25NO4 050657-26-6 5
4 4-n-Butyl-3-[n-octylsulfonyl]nit... 355 C18H29NO4S_ 1000214-51-2 4
Abundance Scan 1974 (14.678 min): 0403LB.D (-1965) (-) m/z 73.10 100.00%
73
5000 267 355
14.40 14.60 14.80 15.00
0- "I m/z 267.00 42.90%
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tet...
73
5000 207 ■ ■ | ■ 1 ' TI .............. | I I । ! | I I
14.40 14.60 14.80 15.00
m/z 355.00 42.75%
133 281 355
0- 4550 ■
103 J [ 177_1 TT1 ,i—ii 2531
i ■ 1 ' ■
. 327 377399 429
| । i n ।ir । i —।। [ i r i —।i —।।pir—ii~ r i Ipr
i ■ 1 1 ■ i 1
489
1 ' i
m/z-> 100 150 200 250 300 350 400 450
Abundance #16941: Codein-propionyl
57
i 1 ‘ 1 ' i ' •
282 14.40 14.60 14.80 15.00
355
5000 81 229 m/z 356.00 15.59%
124 162
। 188
0- • ■ i ■
1 II II || L l —........... ............................... 1‘T
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #19231:1,3-Benzodioxole-5-ethanamine, 6-[2-(3,4-dimethoxy...
58 14.40 14.60 14.80 15.00
m/z 267.90 10.68%
5000 355
204
0
103 127151181 1 238 265 296
L
ti/z—> 50 100 150 200 250 300 350 400 450 14.40 14.60 14.80 15.00
0403LB.D SCANAPR0902.M Thu Apr 11 13:58:40 2002 Page 3
NYC-WTC_000040191
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