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GCMS blank analysis results for sample AE07633, April 2002

Machine-extracted title · confidence 100%

Detailed concentration data for volatile organic compounds in sample AE07633 analyzed between April 3 and 10, 2002.

NYC-WTC_000040186–000040192

Folder label: “GCMS X 4/3/02 A 4/10/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020410\0403LB.D Vial: 3 Acq On : 10 Apr 2002 12:20 pm Operator: Nefliu Sample : 04/03 lab blk Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1. .. \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Heptasiloxane, 1,1,3,3,5,5,. Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.68 0.33 ug/1 270199 Naphthalene-d8 15.76

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9 9 2 Codein-propionyl 355 C21H25NO4 065644-90-8 5 3 1,3-Benzodioxole-5-ethanamine , 6... 355 C21H25NO4 050657-26-6 5 4 4-n-Butyl-3-[n-octylsulfonyl]nit... 355 C18H29NO4S_ 1000214-51-2 4 Abundance Scan 1974 (14.678 min): 0403LB.D (-1965) (-) m/z 73.10 100.00% 73

5000 267 355

14.40 14.60 14.80 15.00 0- "I m/z 267.00 42.90% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tet... 73

5000 207 ■ ■ | ■ 1 ' TI .............. | I I । ! | I I 14.40 14.60 14.80 15.00 m/z 355.00 42.75% 133 281 355 0- 4550 ■ 103 J [ 177_1 TT1 ,i—ii 2531 i ■ 1 ' ■ . 327 377399 429 | । i n ।ir । i —।। [ i r i —।i —।।pir—ii~ r i Ipr i ■ 1 1 ■ i 1 489 1 ' i m/z-> 100 150 200 250 300 350 400 450 Abundance #16941: Codein-propionyl 57 i 1 ‘ 1 ' i ' •

282 14.40 14.60 14.80 15.00 355 5000 81 229 m/z 356.00 15.59% 124 162 । 188 0- • ■ i ■ 1 II II || L l —........... ............................... 1‘T m/z-> 50 100 150 200 250 300 350 400 450 Abundance #19231:1,3-Benzodioxole-5-ethanamine, 6-[2-(3,4-dimethoxy... 58 14.40 14.60 14.80 15.00 m/z 267.90 10.68%

5000 355

204 0 103 127151181 1 238 265 296 L ti/z—> 50 100 150 200 250 300 350 400 450 14.40 14.60 14.80 15.00

0403LB.D SCANAPR0902.M Thu Apr 11 13:58:40 2002 Page 3

NYC-WTC_000040191

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NYC-WTC_000040191Source: NYC Law Department, mirrored locally

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