GCMS surrogate recovery data for sample AE07635, April 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020410\07635.D Vial: 14 Acq On : 10 Apr 2002 10:34 pm Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 **************************** * ** * * * * * **** * * *** ** ********************** Peak Number 3 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 14.69 0.53 ug/1 483406 Naphthalene-d8 15.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 3 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9 40 4 Phenethylamine, N-methyl-.beta. ,... 399 C18H37NO3Si3 010538-85-9 38 Abundance Scan 1976 (14.689 min): 07635.D (-1957) (-) m/ z 73.10 100.00% 70

5000 267 355 ................ 1 ’ I ' 1 1 • I 1 1 40 14.40 14.60 14.80 15.00 0 ---------- m/z 2 67.00 42.80% miz— > 50 100 150 200 250 300 350 400 450 Abundance #115273: Cyclopentasiloxane, decamethyl- 73

5000 267 1 1 1 1 1 1 ' I ’ 1 ................ T 1 TT ' ■ > । i ■ 14.40 14.60 14.80 15.00 355 m/z 3 55.10 40.73% 45 0 , 1 ‘J 1 I1 96 133 165 1932 344429293 323 Td 1 1 ' 1 1 ■ ' ' I 1 1 1 ' I miz-> 50 100 150 200 250 300 350 400 450 Abundance #115315: Cyclopentasiloxane, decamethyl- 70 T-T-p—r-r-r-|-r-r t I 1 1 1 1 | ' 1 355 14.40 14.60 14.80 15.00 267 5000 m/ z 3 56.10 14.76%

45 , 207 323 0- i . i -_ _—J—J_ J_ P a, ' i - 4 i— ■ 1 । ■ ■ ■ 1 i 1 1 1 ' i m/z-> 50 100 150 200 250 300 350 400 450 Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,77,9,9,11,11,13,13-tet... 70 14.40 14.60 14.80 15.00 m/z 268.00 12.87% 5000 207

133 281 355

m/z-> 0 4550 103 177 1 !. 253 _ 377399 429 . . l ' ' ■ 1 1 1 1 1 ri 1 ' 1 1 I ' ' " ' i 1 1 1 r 'P ' ' 1 I 1'1 ’ ' I 1 100 150 200 250 300 350 400 450 489 TII 14.40 14.60 14.80 15.00

07635.D SCANAPR0902.M Thu Apr 11 14:48:18 2002 Page 5

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