GCMS analysis results for sample AE08489, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020419\08488.D Vial: 25 Acq On : 20 Apr 2002 7:45 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 1-Propyne Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.30 0.53 ug/1 659647 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Propyne 40 C3H4 000074-99-7 3 2 Formic acid, propyl ester 88 C4H802 000110-74-7 1 3 1,2-Propadiene 40 C3H4 000463-49-0 1 4 Acetic acid, hydroxy- 76 C2H403 000079-14-1 1 Abundance • Scan 548 (6.299 min): 08488.D (-547) (-) m/z 40.10 100.00% 40

5000

■ ■ ■ i • 1 ■ ■ i ■ - - ■ i • ■ ■ ■ i ■ ■ ■ ■

43 6.00 6.20 6.40 6.60 __ 36 111 - -i'1 ■ • i1B i ■1'11'■ J 47 ‘1 ‘ i “ ■ 'i TTTTTpTnTyrTTTp-rTTJTTTTpnTTY^ m/z 43.10 11.75% iz-> 5 10 15 2025 30 35404550556065 70 75 80859095 Abundance #1402:1-Propyne 40

5000 6.00 6.20 6.40 6.60 37 m/z 36.05 5.96% 13 2528 1 f , .., I .. .. 1.,.. 1 ,. . , I , , ,. 1 ,, , I!,,,,! > 11,1,1, 11 rri 111 n > | 11 ...!. I 111... , I. ., 1111 >, I.... I 111 111 niz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #108322: Formic acid, propyl ester 31 ' ‘ ‘ i ' ' ■ • i ■ ' ‘ ’ i 1 ■ - ■ i ■ ■ ■ ■

42 6.00 6.20 6.40 6.60 5000 m/z 47.00 3.13% 27

n/z-> U ..n... IiI,ii.,i..^iIi.,4/. ....... .... . 5 10 15 20 25 3035404550556065 70 75 80859095 Abundance #1401:1,2-Propadiene 4b 6.00 6.20 6.40 6.60

5000— 37

Irr m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

08488.D SCAN020418.M Thu May 02 12:03:37 2002 Page 4

NYC-WTC_000048679