GCMS analysis results, sample AE07512, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07512.D Vial: 8 Acq On 4 Apr 2002 1:30 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Propiolonitrile Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.31 0.14 ug/1 74188 1,4-Dichlorobenzene-d4 10.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Propiolonitrile 51 C3HN 001070-71-9 3 2 2-Formylhistamine 139 C6H9N30 1000132-95-8 1 3 2-Butyn-l-ol, 4-methoxy- 100 C5H802 018857-03-9 1 4 2-Butyne-l,4-diol 86 C4H602 000110-65-6 1 Abundance Scan 40 (3.314 min): 07512.D (-38) (-) m/z 51.00 100.00% 51

5000 86 M/MMapat I " " I " 1' I " 111 3.20 3.30 3.40 3.50 3.60 3.70 01 ' i' ■ . 11 1 " < । । । । । । . m/z 86.00 66.08% m/z-> Abundance 10 20 30 40 50

51 60 70 80 #12371: Propiolonitrile 90 100 110 120 130 140 .MMWanaul 5000 11111' " i11" i ■1" । " " i" 1 ■ i " ■ ■ । 3.20 3.30 3.40 3.50 3.60 3.70

12 25 38 01 - -Hi-. ,,,!■!•.. f ' ' ■ I ' ' ■ ' | 1 ' ■ - | ■ l ■ ■ ■ ■ | 1 ■ । | ■ 1 । ' | 1 i ' ' l rrrr|-n m/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #10720: 2-Formylhistamine 44 '1 r 1 ‘' i'' " i'1 " i " " I " 111 " '11 3.20 3.30 3.40 3.50 3.60 3.70 5000 m/ z 4 9.10 24.56%

Of ....... , I +H 51 58 69 77 84 95 1 i ‘ ■ ■ r i ■ ■ 1 1 i ' ■ 1 ‘ i1 ■ i। ■11 ■ । 138 1 ■ i111111111111111111 ri11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1255: 2-Butyn-1-ol, 4-methoxy- ■ ■ i ■ ■11 r '111 ■1'111'11111 rri11'11 39 3.20 3.30 3.40 3.50 3.60 3.70 29 69 57 5000 85 50

m/z-> 0 -lll11 10 20 30 40 +PTT+ 60 4+77+4 9092 99100 110 120 130 140 70 80 •J • ■ ■ 1 j ■ । ■ i > ■ ■ ■ I । > > > 11 ■ ■ > I ' >

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