GCMS analysis results for unknown compounds, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\060702\12737.D Vial: 13 Acq On 7 Jun 2002 6:21 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 Propiolonitrile Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 3.81 3.82 ug/L 2114250 1,4-dichlorobenzene-d4 9.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Propiolonitrile 51 C3HN 001070-71-9 7 2 Ethane, 1,1-difluoro- 66 C2H4F2 000075-37-6 4 3 Pyridazine 80 C4H4N2 000289-80-5 2 4 2-Butyne-1,4-diol, diformate 142 C6H604 036677-73-3 1 Abundance Scan 124 (3.808 min): 12737.D (-123) (-) m/z 51.10 100.00% 51

5000 47 86 37 41 3.40 3.60 3.80 4.00 4.20

iz-> 0- Tr i"" r "' i" " i" "i —++ 83 — “' i'"' r ■" i" "I ■ ‘ "I"" i1 THTT 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 m/z 86.00 27.77% Abundance #12371: Propiolonitrile 51

5000 3.40 3.60 3.80 4.00 4.20 m/z 47.00 27.02%

n/z-> Abundance 0- ..1018.28,32,138.47. aHOTTT 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 #111062: Ethane, 1,1-difluoro- _ P*A.. *ww 51 3.40 3.60 3.80 4.00 4.20 5000 65 m/z 50.00 21.58%

miz-> 0- 2 ■"'11" “111 -4 ..................... 47

0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ' ‘ ■ ■ i ■ ■ “ i ■ “ ■ i ■ ■ ■ ■ i “ “ i" ■ • i d*My Abundance #111060: Pyridazine 51 3.40 3.60 3.80 4.00 4.20 m/z 41.00 19.51% 5000 26 80 MA/MY"Am 37

n/z-> 0 " i" " i'" ■ i‘"' i ■ i ■ -Hhm ryoyaasgaagagm — 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 3.40 3.60 3.80 4.00 4.20

12737.D 060302.M Mon Jun 10 11:23:54 2002 Page 5

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