GCMS analysis results for sample AE07978, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020415\07978.D Vial : 18 Acq On : 16 Apr 2002 12:44 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

3.67 0.26 ug/L 227257 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 91 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 72 3 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 25 4 Allyl mercaptan 74 C3H6S 000870-23-5 9 Abundance Scan 100 (3 667 min) 07978 D (-95) (-) m/z 74.20 100.00% 74

82 5000

47 A i 35 40 3.40 3.60 380 4 00 — 01 ' I 1 ' ' ' I • ' m/ z 82.10 51.92% n/z- > 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338 Acetonitrile, dichloro- 74

5000 82 ............................................. 47 3.40 3 60 3 80 4.00 m/z 76.20 32.20% 35 12 ol /111* 26, 1,40 111 i ' 1 * । । । 1 ' I , 62....... । ' | 1 1 1 Tr I’IIU . 108 1 1 I 1 1"mI III11’ n/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342 Acetonitrile, dichloro- 74 35 — 340 3.60 3 80 4 00 5000 82 m/z 84.20 29.48%

0) 40 — 47 MkpmwuWow 11 1 1 1 1 । I 1T5 ' । " । ' i ' 1 ‘ 1 i 1 1 1 i ' ' ' 1 i 1 ■ 1 1 i • ■ 1 1 i n/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28312 3,3-Dichloropropyne 74 340 3 60 3 80 4 00 m/z 47.20 23.38% 5000

0 11 28 38 47 | । 53 60 | 82 ‘In—*nI***IIIIIIIIIIIH 108 "WWwp Lw n/z-> 10 20 30 40 50 60 70 80 90 100 110 340 3.60 3.80 4 00

07978.D 041202SCAN.M Tue Apr 16 13:47:45 2002 Page 4

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