GCMS analysis results for sample AE08067, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08067.D Vial: 24 Acq On : 16 Apr 2002 5:36 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Acetonitrile, dichloro­ Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

3.62 0.31 ug/L 170749 1,4-Dichlorobenzene-d4 9.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

•1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 90 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 3 Allyl mercaptan 74 C3H6S 000870-23-5 9 4 Ethyl ether_____ 74 C4H10O 000060-29-7 4 Abundance <Scan 92 (3,620 min): 08067 D (-86) (-) m/z 74.20 100.00% 74 I 5000 82

47

n/z- > Abundance 01 ....... 1° H 10 20 30 35 ,

40 50 60 ■ i ' 1 1 1 i ■ 70 #28338: Acetonitrile, dichloro- i 1g ■ i ■ 1 ■ 1 i ' 1 ‘ 1 i ' 1 ■ ■ i 90 100 110 3.20 m/z 3.40 3.60 82.10 3.80 4 00 48.55%

74

5000 47 82 3 20 AW.. . 3 40 ' 3 60 380 4.00 ' m/z 84.20 31.10% 35

n/z— > 0+ 10 12 1.2., 20 30 1,19, 40 IV 50 ...6062....70 ' "Il 80 , ' ■ । ■ ■ ■ 1 । • 1 ■ 1 i ' ■ ■ ■ । 90 100 108 110 MpdHWMo Abundance #115342' Acetonitrile, dichloro- 74 35 3.20 3.40 3 60 3.80 4.00 5000 82 m/ z 76.20 29.58% 47 0 0+ 1 ' I ' 1 ' ' I ' ■ ' ‘ I ' 'I I I 4l) 1 ■ 1 ■ । ■ ' ■ ■ । ■ TI3 n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28161 Allyl mercaptan ....... . 41 74 3.20 3.40 3 60 3 80 4.00 m/z 47.20 24.40% 5000

47 MM/ W yMMww n/z-> 0 27 -1 1 1 1 I ' I t I I I I l 10 20 30 33 I

40 1,5359 69, 50 60 70 l t ' ■ i 80 ■ ■ ' ■ i 90 ■ ■ ■ 1 100 i ' • ' 1 110 i 1 ■ ■ ■ i

3 20 3.40 3.60 3.80 4 00

08067.D 041202SCAN.M Tue Apr 16 13:56:07 2002 Page 4

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