GCMS analysis results for sample AE07975, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020415\07975.D Vial: 15 Acq On : 15 Apr 2002 10:15 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 Acetonitrile, dichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

3.68 0.42 ug/L 354351 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 3 Allyl mercaptan 74 C3H6S 000870-23-5 9 4 Thiirane, methyl- 74 C3H6S 001072-43-1 7 Abundance Scan 102 (3.679 min) 07975 D (-96) (-) m/ z 74.20 100.00% 74

5000 82

47 ------------- 38 3.40 3 60 3.80 4 00 ______________ lull —— 0+ I ------------------- m/z 82.20 49.04% Tl/Z-> Abundance i ■ 1 ■ ■ i ' ■ ' ' i ■ ■ ' ‘ 1 1 10 20 30 40 50 ■ I ■ ' ' ' I 1 60 70 1g 90 100 110 I #28338' Acetonitrile, dichloro- 74

5000 82 A... 3.40 3.60 3.80 4.00 47 m/z 76.20 33.46% 35 Ot 12 TPPm— 26 —L . . 62......... 1 ' ' i 1 ' ' ' i 1 . ■ । I ■> l ■ । 108 • 1 । 1 ■ 1 1 I ■ ■ • ■ । 1 Tl/Z--> 10 20 :30 40 50 60 70 80 90 100 110 Abundance #115342 Acetonitrile, dichloro- 74 35 — 1 ■ i r ■ ■ ■ i ' 3.40 3.60 3.80 4.00 5000 82 m/ z 84.20 32.54% 47 40 0+ ' ' I ' ' ' ' I ' ' ' ' I 1 ‘ — ■ ' । ' 1 11' WWW __ n/z— > 10 20 30 40 50 60 70 80 90 100 110 Abundance #28161 Allyl mercaptan 4f1 74 340 3.60 380 4.00 m/z 47.20 20.19%

Ti/Z-> 5000

0 10 27 33 , oopoeepam 20 30 47

44153.58_ #11 40 50 60 69 ,

70 । ■ । ■ ■ ■ ■ 80 । ■ ■ ■ ■ । < 1"" । । । । । 90 100 110 j3.40 3 60 MMWwwWMrow

3.80 4 00

07975.D 041202SCAN.M Tue Apr 16 13:45:21 2002 Page 6

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