GCMS analysis results for sample AE07975, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020415\07975.D Vial : 15 Acq On 15 Apr 2002 10 :15 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 2 Methane, bromodichloro- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

3.40 0.29 ug/L 238724 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 90 2 Methane, bromodichloro- 162 CHBrC12 000075-27-4 74 3 Methane, oxybis[dichloro- 182 C2H2C140 020524-86-1 64 4 Methane, bromodi chloro-162 CHBrC12 000075-27-4 64 Abundance Scan 55 (3 402 min) 07975 D (-47) (-) m/z 83.20 100.00% 83

5000

47 ---------------------------------------------------------- 129 3 20 340 3.60 3.80 35 |, ol —11—0 ■ । “111" 1' Hi' 1123..— ........... Il,....................... m/z 85.20 66.88% n/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 #116506 Methane, bromodichloro- I 83

5000 —A 3 20 3.40 3 60 3 80 47 129 m/z 47.20 18.24% 35.. III. 55 64 72 | | I9,1, 116 11 144 163 _ 13 01 111'''11111 " 1111111'1111111111'111111 11 1*mu—uu*nDTOnm n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116496 Methane, bromodichloro- 83

3 20 3.40 3 60 3.80 m/z 48.20 14.81%

A 5000

47 129

n/z-> 13 ol 11....... Ip 1'11,11111 58 —4 494 70 1'1'' 11 L_ 164 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 116 rm-j-r

Abundance #33237 Methane, oxybis[dichloro- 83 3 20 340 3.60 3.80 m/z 129.10 12.83% 5000 47 28 0 TTT 37 viln ..... 70^ 11,|.............. ......................................... i rpmI +rr Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3 20 3.40 3 60 3.80

07975.D 041202SCAN.M Tue Apr 16 13:45:19 2002 Page 5

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