GCMS analysis results for sample AE07975, April 18, 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020415\07975.D Vial: 15 Acq On 15 Apr 2002 10:15 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 1 Heptane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 3.17 0.50 ug/L 418685 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane 100 C7H16 000142-82-5 76 2 Heptane 100 C7H16 000142-82-5 64 3 Heptane 100 C7H16 000142-82-5 64 4 Heptane 100 C7H16 000142-82-5 50 Abundance Scan 15 (3 167 min) 07975.D (-8) (-) m/z 57.30 100.00% 43 57

5000 71

86 100 35 3 20 3.30 340 3.50 3.60 -- 0- 49 I I m/ Z 43.30 89.23% n/Z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #109668. Heptane 43

5000 57 71 YITBupuri ., 29 3.20 3.30 3.40 3 50 3.60 71.30 48.31% 100 —37L40 +514 22 | 63 77 85 91 । 0- ।' —---t PT— 1 I 1 ■ 1 ■ i"' 1*1111/1/1/1/1/1,1,11 n/z- > o 10 20 30 50 I60 70 80 90 100 Abundance #4133: Heptane 43 1 1 1 ' 1 ' I ' 1 ' 1 1 1 -P 3 20 3 30 340 3.50 3.60 5000 29 57 71 m/z41.30 46.47%

100 15

n/z-> 0- 2 II—IT - — 0 10 20 30 11 40 +5114 50 PT ।60 65 11 < 1111 85 70 80 >■ 11111 90 ■ । r। 100 TTF

Abundance #109303: Heptane , MAAMA 43 3 20 3 30 3 40 3 50 3.60 m/ z 56.30 31.04% 5000 29 57 71

100

n/z—> 0 1 15 i ■ ■ ■ 1 i ■ ■' ■ ■ । 0 10 20 4434,40 +5114 30 50 T I60 65 11771185.... 1. 70 80 90 100 "IT Aw.... |... . 3 20 3 30 3.40 3.50 3.60

07975.D 041202SCAN.M Tue Apr 16 13:45:16 2002 Page 4

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