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GCMS analysis results for sample AE08253, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08253 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047830–000047850

Folder label: “GCMS X 4/8/02 A 4/17/02

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Scanned page image, NYC-WTC_000047839
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08253.D vial: 11 Acq On : 17 Apr 2002 5:42 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Heptane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

3.15 0.30 ug/L 327364 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane 100 C7H16 000142-82-5 72 2 Heptane 100 C7H16 000142-82-5 72 3 Heptane 100 C7H16 000142-82-5 64 4 Heptane 100 C7H16 000142-82-5 64 Abundance Scan 13 (3.156 min): 08253.D (-4) (-) m/z 43.10 100.00% 4(3 57

71 5000

100 1 1 i ' I1 1 ' 1 I ' r 86 3.20

m/z-> 0- -l +50 0 10 20 30 40 50 60 70> g 80 90 100 - m/z57.10 3.30 3.40 3.50 76.14% 3.60

Abundance #109598: Heptane 4(3

5000 57 11.T 29 71 3.20 3.30 340 3.50 3.60 m/z 71.10 53.57% 100 A m/z-> 0 ......... I' 1 1 ' I ' ' m'l ' ' 37, 0 10 20 30 40 +51 50 60 63 70 I I I I I I' — 85 1 1 । 1 ■ ■ 1 । 80 90 ■ 100 Abundance #4133: Heptane 4(3 A yA I I I I [ t I I I I I I I I I I I I I I I /A I II I r r

3.20 3.30 3.40 350 3.60 5000 29 57 71 m/z 41.10 46.62%

15 100 2 65 - | I । ' । I ■ ■85‘ 1, 20I — I । । 51 1 o1 T87 ' — । ■ 1 ' 1 | ■' TId m/z--> 10 30 40 50 (60 70 80 90 100 Abundance #109668: Heptane TII NT ।11 4(3 3.20 3.30 3.40 3.50 3.60 m/z 56.10 39.58%

5000 57 71 29

0 22 | -37440 1 1 I 1 ' 1 1 i ' ■ ■ ■ i ■ ■ 1 1 1 1 ,51,|||, 63 PT 77 — 91 85 1°0 । / L ।_ , । r1 1 1 1 i 1 1 m/z--> 0 10 20 30 50 (60 70 80 90 100 3.20 3.30 3.40 3.50 3.60

08253 .D 041702SCAN.M Fri Apr 19 08:37:58 2002 Page 6

NYC-WTC_000047839

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NYC-WTC_000047839Source: NYC Law Department, mirrored locally

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