GCMS analysis results for sample AE07976, April 18, 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020415\07976.D Vial: 16 Acq On 15 Apr 2002 11:05 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 1 Heptane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

3.14 0.21 ug/L 165372 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptane 100 C7H16 000142-82-5 80 2 Heptane 100 C7H16 000142-82-5 80 3 Heptane 100 C7H16 000142-82-5 80 4 Heptane 100 C7H16 000142-82-5 53 Abundance Scan 11 (3 144 min). 07976 D (-4) (-) m/z 43.30 100.00% 43 / 71 57 5000

100 _________ AAA AM/Y ' 1 1 1 I ' ' ' 1 I 11 ' ’ 1 ‘ 50 3.20 3 30 3.40 3 50 3.60 88 0- I ' ■ ■ 1 i r ■ ■ ' i ' 1 1 1 1 1 ' ' 1 I L "yil 00//——/— ‘ I m/z 71.30 71.49% n/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #109303: Heptane 43

5000 29 57 71 3.20 3.30 3 40 3.50 3 60'

X.. m/z57.30 63.70% 100

-n/z—> 0- 0 1 15 1 111 1'' ' । 1 10 20 —34 +511— -m 30 40 50 60 65 70 77 80 85 90 I 100 ""I

Abundance #109668 Heptane 43

3 20 3 30 3.40 3 50 3.60 5000 57 71 m/z 41.25 58.87% 29

100

n/z— > 0- 22 T' ' 1 ' . ................. ' o 10 20 371 t11 ’ ■' ' I :30 40 511 50 60 63 ,1,7785,91.., 70 80 90 100 Abundance #109598 Heptane T‘‘T i 1 I t V. rf 11 43 3 20 3.30 3.40 3.50 3 60 m/z 56.30 39.83%

5000- 57 29 71

100

n/z-> 0 0 ■' । । 1 । 1 । । 1 1 1 । 10 20 :30 34 50511 40 60 63 'I 1 r 111111 70 80 85 90 100 3 20 3.30 3.40 3 50 3 60

07976.D 041202SCAN.M Tue Apr 16 13:46:03 2002 Page 4

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