GCMS analysis results for sample AE07976, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07976.D Vial: 16 Acq On : 15 Apr 2002 11 :05 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Acetonitrile, dichloro­ Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 3.66 0.32 ug/L 249702 1,4-Dichlorobenzene-d4 9.99 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 90 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 72 3 Allyl mercaptan 74 C3H6S 000870-23-5 9 4 Thiirane, methyl- 74 C3H6S 001072-43-1 7 Abundance Scan 100 (3.667 min): 07976 D (-95) (-) m/z 74.15 100.00% 74

82 5000

0+ 47

I। ... /s..... m/z 340 3 60 82.20 3 80 4 00 56.28% ■ ■ i ■ ' ■ > । Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338' Acetonitrile, dichloro- 74

5000 82 .0 47 3.40। 3.60 3.80 4.00 35 m/ z i76.20 37.72%

n/z-> 0 12 TTHm 10 20 26,4440, l 30 40 50 60 ., 62......... , ■ ■ । ■ ■ ■ ■ । ■ 70 80 , *-Immi i-i । । । । i'| । । 90 100 108 110 Abundance #115342 Acetonitrile, dichloro- 74 35 ................ . 340 3.60 3.80 4.00 5000 82 m/ z 84.20 34.75% 47 40

n/z- > 0+ • ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 ' 10 20 30 IL 40 ''I ' ' 1 1 I 1 1 1 1 I 1 50 60 70 80 ' I ' ' ' 1 I ' ' ' ' I ' 1 ' ' I 90 100 110 Abundance #28161: Allyl mercaptan TI 4n 74 3 40 . 3.60 3.80 4 00 m/ z 47.20 25.65% 5000

0 2/ 33 । 47 s3 59.69 ' 1 1 1 I ' ' 1 1 I ' ' « II ■ i ■ - ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ । ■ ■ ■ ■ । 4u Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 3.40 3.60 3 80 4 00

07976.D 041202SCAN.M Tue Apr 16 13:46:06 2002 Page 5

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