GCMS analysis results for sample AE07976, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020415\07976.D Vial: 16 Acq On : 15 Apr 2002 11:05 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 N,N-Dimethylacetoacetamide Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

5.15 0.26 ug/L 200884 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N,N-Dimethylacetoacetamide 129 C6H11NO2 002044-64-6 47 2 Hexanal 100 C6H120 000066-25-1 27 3 Hexanal 100 C6H120 000066-25-1 12 4 Hexanal 100 C6H120 000066-25-1 12 Abundance Scan 352 (5 147 min): 07976.D (-347) (-) m/z 44.25 100.00% 44 129 56

5000 72 82 50 4.80 5.00 5.20 5.40_____ 0+ 11 . II r 1111 1 ■ । ■r1 1 ■ ।1 ■ ■ ■ । m/z 129.10 86.98% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #110552: N,N-Dimethylacetoacetamide 44

5000 1 i ■ ' 1 ' i '

72 129 4.80 5.00 5.20 5.40 15 m/z 41.30 69.39% ■ .30 38 | co 58 85 | 101 114 0+ ■ । ■1 I* I ' ' ^T' ' ' 'T1 I59—4... 'J ■ < ■ I ■ I 'I'1 | < ■ 1 1 l'1 1 i । । f I ' । । i—•—r' | । । । > । n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130

A Abundance #10785: Hexanal 41 56

4 80 5.00 5.20 5.40______ 5000 29 m/z 56.30 69.39%

72 82

Tl/Z-> 0+ 7. 14.39/ 10 20 30 40 50, | 65.1 | 94 100 1 ■ i 11 1 । i 1 1 ■ ''| l ' ■ 1 Ii . . । । । । 50 60 70 80 90 100 । ।। ।। ।। ।। । । 110 120 130 Abundance #110563. Hexanal ■ i ' ■ • ' i 1 ' • • i ■ ' 1 ■ i 1 41 4.80 5.00 5 20 5 40 56 m/z 43.30 66.92% 27 5000

72■ 82 0- . 10....... 111371, —4 |1 50 1 i ■ ■ ■ i 1 - A Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 4.80 5.00 5 20 5.40

07976.D 041202SCAN.M Tue Apr 16 13:46:09 2002 Page 6

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