GCMS analysis results for sample AE07977, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\l\DATA\020415\07977.D Vial: 17 Acq On 15 Apr 2002 11:54 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 4 N,N-Dimethylacetoacetamide Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 5.16 0.30 ug/L 269403 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N,N-Dimethylacetoacetamide 129 C6H11NO2 002044-64-6 35 (2) Hexanal 100 C6H120 000066-25-1 27 3 Hexanal 100 C6H120 000066-25-1 27 4 Hexanal 100 C6H120 000066-25-1 27 Abundance Scan 354 ( 5.159 min) 07977.D (-349) (-) m/z 44.25 100.00% 41 56 129

5000 72 82 semonwricy —mr 4.80 5 00 5 20 5.40 5.60 ■ i ' 1 ' ' i ' 1 • 1 i 1 ' 1 III 1 < < i ■ ■ ■ ' i ■ ■ - ■ । ' । ■ 1 ■ । ' । 01 rl ' 1 TI...... i' । I* m/Z 129.10 90.22% n/z-> Abundance 10 20 30 40 50 60 70 90 80100 #110552: N.N-Dimethylacetoacetamide 110 120 130 y 44

5000 72 129 4 80 5 00 5 20 540 5.60 m/ Z 56.30 87.79% 85

n/z--> 0+ „... 32.88, 1?..?. ,1 10 20 30 40 50 60 70 1.1 101 114 Tpr r i . ............... I ■ ■ I ■ ■ । .‘l ■ ■ ■ ’ l 80 90 100 110 120 130 Abundance #110561: Hexanal 41 56 4 80 5 00 5 20 5.40 5.60 5000- 27 m/z 41.25 87.19%

72 82

Tl/Z-> 01 ' ■ i ■ ■ ■ ■ i • ■ 10 20 i —t, 1 30 38 40 — 50 | 50 +62 60 11 70 80 98 90 100 110 120 130 Abundance 41 #110563 Hexanal 1 4.80 5.00 5.20 5.40 5.60 56 m/ z 57.30 67.78% 27 5000

72

n/z- > 0 • • i • । ■ I 1 । • । I । । ■ 37 10 20 30 M’I’n 40 15, 50 + 60 70 80 90 100 i ' 1 ' 1 i 1 ' 1 ’ i 1 ' 1 1 i 110 120 130 4 80 5 00 5 20 5.40 5.60

07977.D 041202SCAN.M Tue Apr 16 13:47:09 2002 Page 7

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