GCMS analysis results for sample AE08065, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020415\08065.D Vial: 22 Acq On 16 Apr 2002 3:59 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 N,N-Dimethylacetoacetamide Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 5.14 0.23 ug/L 198774 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N,N-Dimethylacetoacetamide 129 C6H11NO2 002044-64-6 43 2 Thiophene, 2 -nitro- 129 C4H3NO2S 000609-40-5 37 3 Hexanal 100 C6H120 000066-25-1 22 4 Hexanal 100 C6H120 000066-25-1 12 Abundance Scan 351 (5 142 mm) 08065.D (-346) (-) m/z 44.25 100.00% 44 129 56

5000

35 72 82 wnmhm lhemuartan 4.80 5 00 5 20 5 40

m/z—> 01 10 20 30 1 40 50 60 70 80 90 100 H 110 120 130 140 m/z 129.10 86.21% Abundance #110552' N,N-Dimethylacetoacetamide 44

5000 1 ' i ■ ■ ■ ■ i ■

129 4.80 5 00 5.20 540 72 m/z 41.30 86.04% 15 85

n/z- > 0+ 10 4 11T 3038 ? ”... J .... I|...... 101 . ....... ....... 20 30 40 50 60 70 80 1 • ■ | ■ 1 I I | 90 100 . 1 |‘1 | 1 ' | I I 1 ' | I ' I | ‘|-1-r ! ! | ! 110 120 130 140 Abundance #58233: Thiophene, 2-nitro-

45 55 119 uMMAMtunt 4 80 5.00 5 20 5 40 5000 m/z 45.30 77.96% 99 71 83 113 , , 64 । m/z—> 0+ .. i"'"1 1 1 1 1 1 1 1 1 ' plpaaps) 10 20 30 40 50 60 70 80 T’I—ur 90 r.... 1, " I ' —P 100 110 120 130 140 Abundance #10785: Hexanal 44 Tn 56 4 80 5 00 5 20 5.40 m/ z 43.30 74.89%

5000

MWa 29 72 82

n/z—> 0- --34 10 20 30 40 50,1 651 , 50 60 70 80 94 100 1 ■ । ■11 90 100 110 120 130 140 ।1111111 I A 4 80 5 00 5.20 5.40

08065.D 041202SCAN.M Tue Apr 16 13:54:44 2002 Page 6

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