GCMS results for sample AE08069, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08069.D Vial: 26 Acq On : 16 Apr 2002 7:13 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

3.64 0.25 ug/L 168101 1,4-Dichlorobenzene-d4 9.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 91 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 43 3 Allyl mercaptan 74 C3H6S 000870-23-5 9 4 Thiirane, methyl- 74 C3H6S 001072-43-1 9 Abundance Scan 95 (3 637 min) 08069 D (-91) (-) m/z 74.20 100.00% 74

82 5000 47 35 . ■ ..................

3 20 340 3.60 3 80 4 00 0+ ........ I, '| I J . J li. L ' I ■ ■ 1 I I ■ ■ 1 I I 1 I > 1 I m/ z 82.20 54.12% Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 ... A... I.w ...... . 3 20 3.40 3 60 3.80 4.00 47 m/z 76.20 33.14% 35

/z- > 01 10 12 —2—4H0, 20 30 40 50 62 60 ’ ’ I ’ 70 I , FTmTNTTTT 80 90 100 108 110 Abundance #115342: Acetonitrile, dichloro- 74 35 3.20 3.40 3 60 3.80 4.00 5000 82 m/z 84.20 25.95%

40 47 MMLaAsposd/VAMoopoas 01 I ■ ■ ■ ’h 1 1 1 1 i 1 ' 1 1 i '' ■ ■ i < • • • । • i ' > l TTI 1 ' । ■ । ■ ' ■ ' । ' ' ' ' । n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28161' Allyl mercaptan 41 74 3.20 3 40 3.60 3.80 4.00 m/z 47.20 22.89% 5000

0 -lll 1153 27 33 । 47 59 -4 ■ i ■ ■ ' ■ i ■ ■ ■ ■ । । 1 1 ■ i ■ ■ ■ ■ । -ww WMMMWryw n/Z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3 60 3.80 4.00

08069.D 041202SCAN.M Tue Apr 16 13:58:30 2002 Page 4

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