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GCMS results for sample AE08069, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08069 including surrogate recovery and unknown compounds on April 18, 2002.

NYC-WTC_000046841–000046854

Folder label: “GCMS X 4/5/02 A 4/16/02

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Scanned page image, NYC-WTC_000046849
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08069.D Vial: 26 Acq On : 16 Apr 2002 7:13 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Hexanal Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.13 0.23 ug/L 159082 1,4-Dichlorobenzene-d4 9.98

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanal 100 C6H120 000066-25-1 12 2 Hexanal 100 C6H120 000066-25-1 12 3 Boron, trihydro(N-methylmethanam... 57 C2H8BN 000074-94-2 10 4 Ethene, ethoxy-72 C4H80 000109-92-2 9 Abundance Scan 349 (5 130 min) 08069 D (-343) (-) m/z 56.30 100.00% 41 56 129 5000 72 48 82 4 80 5 00 5 20 5 40 0- । 1 ■ • ■ i ■ 1 ■ ■ i m/z 41.30 98.13% n/z-> Abundance o 10 20 30 40 50 60 70 80 #110561 Hexanal 90 100 110 120 130 A 44 56

5000 27 MMuI I 4.80 5 00 5 20 540 72 m/ z 44.30 89.57% 82 — 50 | । 62 । । - 98 n/z-> 0- 0 10 20 30 40 —t 50 ‘ I 1 1' 1 r11 60 70 Tmmru I | I ! I ! | I I ! I | I 80 90 100 110 120 130 Abundance #10785: Hexanal 41 56 ilMWwWW 4 80 5 00 5 20 5.40 5000 m/z 43.25 63.64% 29 72 82

n/z- > 0- 0 ■ i • ■ ■ • i ■ 10 20 1341 30 40 50_ 651 50 60 70 L 80 94 100 90 100 110 120 130 ' ' ' ' I ■ ' 1 1 i 1 ' ' ' i ' 1 ' ■ i '

Abundance #109528: Boron, trihydro(N-methylmethanamine)-, (T-4)- 43 55 4 80 5 00 5 20 5 40 28 m/z 40.20 60.56% 5000 13

n/z- > o -— 0 10 1—2022L 30 o+ 40 50 । 50 60 70 80 90 100 110 120 130 4 80 5 00 5.20 5 40 TT

08069.D 041202SCAN.M Tue Apr 16 13:58:30 2002 Page 5

NYC-WTC_000046849

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NYC-WTC_000046849Source: NYC Law Department, mirrored locally

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