GCMS analysis results, Sample AE08265, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08265.D Vial: 22 Acq On : 18 Apr 2002 2:44 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Heptane Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

3.14 0.23 ug/L 254875 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane 100 C7H16 000142-82-5 72 2 Heptane 100 C7H16 000142-82-5 64 3 Heptane 100 C7H16 000142-82-5 59 4 Hexane, 3-methyl- 100 C7H16 000589-34-4 45 Abundance Scan 10 (3 138 min). 08265.D (-3) (-) m/z 43.10 100.00% 43 57 71

5000 100 83 3 20 3 30 3.40 3 50 3 60 — J J............. 0- ""I m/Z 71.10 84.42% n/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #109668: Heptane 43

5000 29 57 71 .M4........... h 3.20 3 30 3.40 3 50 3 60 m/z57.10 84.26% 100 ................ .............................. n/z-> 0- 22 | 37 1 ' I 1 1 1 1 I 1 ' 1 1 I'' 1 11tr ■ re o 10 20 :30 40 +514460 —m 50 ( m 77 85 91 63 1 i ■ 1 70 80 90 | 100 Abundance #4133 Heptane 43 3.20 3.30 340 3.50 3.60 5000 29 57 71 m/z 41.05 60.13%

15 + 100

JosAoc 2 65 85 0 1" i ' । i - ' H1! ■ ' ' 1 Poy ‘II n/z—> 0 10 20 30 40 50 I60 70 80 90 100 Abundance #109303 Heptane 43 3 20 3 30 3 40 3.50 3 60 Z 56.10 47.61%

5000 29 57 71

100

n/z-> 0 ■ ■ i

0 1 ■ ■ ■ ■ i ■

10 15 ■ i ■ ■' ■

20 434 +5114 30 40 50 65 PT 'I । 1II1 I60 70 77 85 . 80 90 I 100 ""T 3.20 3.30 3.40 3.50 3.60

08265.D 041702SCAN.M Thu Apr 18 09:58:13 2002 Page 6

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