GCMS analysis results for sample AE08324, May 2002

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Data File : C:\MSDCHEM\1\DATA\020419\08324.D Vial: 11 Acq On : 19 Apr 2002 5:58 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Methane, bromodichloro- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 3.34 0.27 ug/1 376356 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Methane, bromodichloro- 162 CHBrC12 000075-27-4 83 2 Methane, bromodichloro- 162 CHBrC12 000075-27-4 83 3 Methane, bromodichloro- 162 CHBrC12 000075-27-4 74 4 Chloroform 118 CHC13 000067-66-3 72 Abundance Scan 44 (3.338 min): 08324.D (-41) (-) m/ z 83.00 100.00% 83

5000

40 48 Tpmmfer 129 3.20 3.30 3.40 3.50 3.60 3.70 rr ' MT rmmrln 1r 11191195 I I I | I I II | ! i 1 r [ || | < | ■ i ■ ■ ■1111, ■ । ।11 *11 TUT m/ z 84.95 58.86% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116497: Methane, bromodichloro- 83

5000 An$,AA* PRYwm A M ns 3.20 3.30 3.40 3.50 3.60 3.70 47 m/ z 40.10 19.59% ................... 129 IL 191 _L ■ i'' ■ ■ r ■1 ■ r ■ ■ ■ ■ i‘ ■ ■ 11 -. ■. ।... ■ ।.. ‘‘I‘ ... ।. 11 I ■''' I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance ;#33236: Methane, bromodichloro- 83 TTO—tET0111-—1--I-TEII-TTI1‘11131 3.20 3.30 3.40 3.50 3.60 3.70 5000 m/z 47.10 17.59%

m/z-> Abundance ............... 1.11.63..72. 47

183 ||, 164 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 #116506: Methane, bromodichloro- 116 129 ■ । ■ ■. > । ■ 11 ■ i < ■" । ■ ■.' । ■ ■. ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■' l MMoopoi ww 1' I'''' 11'1' I'''' I''f r I'''' 83 3.20 3.30 3.40 3.50 3.60 3.70 m/ z 48.00 13.18%

5000

47 ,l|i, 55 64 72 ||, , I9,! 35 129 116 11 144 163 VWM MNJyn.A 13 TTUUTTTETTTTTTTTT '111" 111, >■■।>1111 **1***———" /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.20 3.30 3.40 3.50 3.60 3.70

08324.D SCAN020418.M Fri May 03 09:04:33 2002 Page 4

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