GCMS scan comments for sample AE11480, May 29, 2002

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Data File : C: \MSDCHEM\1\DATA\020521\11480.D Vial: 14 Acq On : 21 May 2002 9:12 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 Methane, bromodichloro­ Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 3.35 0.34 ug/1 24823 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 78 2 Methane, bromodichloro- 162 CHBrC12 000075-27-4 78 3 Methane, bromodichloro- 162 CHBrC12 000075-27-4 78 4 Chloroform 118 CHC13 000067-66-3 64 Abundance Scan 46 (3.349 min): 11480.D (-43) (-) m/z 83.00 100.00% 83

5000 4 mA7l MA । n nmon 35 47 129 3.20 3.30 3.40 3.50 3.60 3.70 3.80 Of - .............. || 1' I ‘'1 ‘ I ‘11II’ ।11।।. I""I""I""I"I m/z 84.90 71.53% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #33236: Methane, bromodichloro- 83

5000 _Hy=RHH 3.20 3.30 3.40 3.50 3.60 3.70 3.80 47 m/z 47.05 17.18% 129 o+ " ' l1327 25 -63-72.4+ 13 ' " i'1 " 11 " 111ITTE111 164 116 ||, ' i1''11' " ' i “ ‘11 ■।। ' IT’1 11111 miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116496: Methane, bromodichloro- 83 Wy 3.20 3.30 3.40 3.50 3.60 3.70 3.80 5000 m/z 35.10 13.09% 47 129 35

miz-> 13 01 T'1 ' thri | ITTI | 1-++58—70—4 I9,! 116 14mPpp 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 1L 164 T''111 ■1 ■11" ■' i" " i'1

Abundance #116497: Methane, bromodichloro- 83 3.20 3.30 3.40 3.50 3.60 3.70 3.80 m/z 49.00 13.06% 5000 ImpMMMMhp 28 47 — 129

n/z-> 0 ,1,1377 ...........Ill ............. t.............. " i ""i■ 11'''111 " 11 " ’ । rr. 11 11 । । । 11 111 ■ ।, , j , 11 i । । । । 11 11 i 11 । i । । 11 । 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.20 3.30 3.40 3.50 3.60 3.70 3.80

11480.D SCAN020521.M Fri May 24 09:32:16 2002 Page 3

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