GCMS analysis results for sample AE08323, May 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020419\08323.D Vial: 10 Acq On : 19 Apr 2002 4:59 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Methane, bromodichloro- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

3.33 0.25 ug/1 332843 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 83 2 Methane, bromodichioro - 162 CHBrC12 000075-27-4 78 3 Methane, bromodichloro- 162 CHBrC12 000075-27-4 74 4 Methane, bromodichloro- 162 CHBrC12 000075-27-4 74 Abundance Scan 43 (3.332 min): 08323.D (-39) (-) m/ z 83.00 100.00% 83

5000

47 129 TNTfA 3.20 3.30 3.40 3.50 3.60 3.70 ......... 37 56 71 I 193 T‘I‘‘ET‘TT——IEUIITTTIEITuTT 1 '1'1111' I h "i"" ।■11" " r ‘"i'' " i1 “ ■ i■ ■ "i " 111'' m/z 85.00 76.86% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #33236: Methane, bromodichloro- 83

5000 +=*444444*242440 3.20 3.30 3.40 3.50 3.60 3.70 47 m/ z 47.10 21.12% 129 .13.0727,35.. 1,.163..72.4 1 93 116 ||, 164

vww pt T‘ ' i " " i " 1' i'1 "T' ■11111111111111111111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116506: Methane, bromodichloro- 83 3.20 3.30 3.40 3.50 3.60 3.70 5000 m/z 40.10 15.36%

47 129 13 35 ||i, 55 64 72 11,|, l.l,I9,! । । , , , , । ।116 11 144 163 • ■ i ' I • ■ ■11 ■ ''i ■ । > 1*1010OUTgOnm_uupT , rij 1*****

Tl/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116497: Methane, bromodichloro- 11 ' ’ ' I i " '11'1 ■11 " " 11 " 111 8 3.20 3.30 3.40 3.50 3.60 3.70 m/z 128.90 14.99% 5000

47

/z-> ’ ■ i ■ ■1 ■ i' 10 20 28,27— 11 91 129 ll. ' i1 ■' ■ i ‘ ‘1' T ■ ■ ■ ■ i ■ ■ • • ।1 ’1 ■ i" " r11 ■ i ■ ■ ■ ■ i ■ ■11 r11111111111' 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 " i' " 11 "1 ‘ i " " i " 111 " 1111 " 111 3.20 3.30 3.40 3.50 3.60 3.70

08323.D SCAN020418.M Thu May 02 15:23:50 2002 Page 4

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