GCMS analysis results for sample AE08067, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08067.D Vial: 24 Acq On : 16 Apr 2002 5:36 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Methane, bromodichloro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.33 0.27 ug/L 152008 1,4-Dichlorobenzene-d4 9.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 83 2 Chloroform 118 CHC13 000067-66-3 72 3 Methane, oxybis[dichloro- 182 C2H2C140 020524-86-1 56 4 Chloroform 118 CHC13 000067-66-3 56 Abundance Scan 43 (3 332 min): 08067.0 (-33) (-) m/z 83.20 100.00% 83

5000-

47 p MM $100108. 129 3 20 3 30 3 40 3 50 3 60 3 70 35 I llil II 0 1 ■i " " r' ----- |l90.............. IL ' I ‘‘ ‘ 1 | • I ' I | I 1 r 1 | l ' m/z 85.20 54.87% n/z- > 10 20 30 40 50 60 70 80 100 110 120 130 140 150 160 170 Abundance #116496: Methane, bromodi chloro- 83

5000 .......... I VY .............. n 3 20 3 30 3.40 3 50 3 60 3.70 47 m/z 47.20 17.70% 129

n/z-> 04 Abundance 13 .................... "'ll .-.ih .W 1 91I ' 1 ' I | I I I | | ri116I , | I | I'lll1!1. I ! ! | ! I 111164 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 #116499. Chloroform 1 ■1 ■ ।11 AiW). 8b ■111" ■ । ■' ■ ■ ।1" ■ ।"111"111"1 ■ । ■ 3 20 3 30 3 40 3 50 3.60 3.70 5000 m/z 48.20 12.27% 47 35 | 118 n/z— > 01 ' ■ i ■ ■ ‘ ■ i ■1" I'1111,111"

10 20 30 40 50 . .............. . 111 60 70 80 1 " T" ' I 1 1 PMl । 11 । । i ■ । । 90 100 110 120 130 140 150 160 170 11 ■'1 ■ i1 ■ Mhw VMA/ AP Abundance #33237 Methane, oxybis[dichloro- PTPP 83 3.20 3.30 3.40 3.50 3.60 3.70 m/z50.20 10.02% 5000 47 l . n/Z-> 0- -4ZH. 10 20 28

30 40 50 70 ■ i ■ ■ ■ ■ I • 60 70 80 90 100 110 120 130 140 150 160 170 L_ 111' '' 1 1 1 ■' I'' । ■ ■ ■ ■ । • 3 20 3 30 3 40 3.50 3 60 3 70

08067.D 041202SCAN.M Tue Apr 16 13:56:07 2002 Page 3

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