GCMS analysis results for sample AE08067, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE08067 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046799–000046812

Folder label: “GCMS X 4/5/02 A 4/16/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\DATA\020415\08067.D Vial: 24 Acq On : 16 Apr 2002 5:36 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 Acetic acid ethenyl ester Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

3.76 6.23 ug/L 129507 1,4-Dichlorobenzene-d4 9.98 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid ethenyl ester 86 C4H602 000108-05-4 4 2 Propane, 2-(ethenyloxy)- 86 C5H10O 000926-65-8 4 3 2-Chloroethanol 80 C2H5C10 000107-07-3 4 4 3-Oxobutyric acid, 2-chloroethyl... 164 C6H9C1O3 1000210-13-3 4 Abundance Scan 116 (3 761 min) 08067 D (-106) (-) m/z 43.30 100.00% 43

5000 . A , / A.) ,4wh, ,4 1 i ' 49 85 340 3 60 3 80 4 00 4.20 35 40 n/z- > 0- TTT IUBINURUmungu 0 5 11417,1... 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 "i"' m/ z 41.30 11.54% Abundance #109145 Acetic acid ethenyl ester 43

5000 3.40 3.60 3.80 4.00 4 20 m/ z 44.30 10.43%

AjBmiow 27 5760 71 86 n/z-> 0- „0 .............. 1.31..374Q1 , 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 11" " 1" " 1" " 1 ” " 1" ” 1' ‘" 1" " 1" " 1'"11" " 1 ■"

Abundance #4753 Propane, 2-(ethenyloxy)- 43 340 3.60 380 4 00 4 20 27 5000 m/z 49.20 7.99% 15 39 58 86 MWwdyMMMMo 0- 2 121 19 241 31 36, , I >| I ll I | H If| I III | I I I | I I I I | I I I | | 46495255 1,61 687174 83 89 11" ' I " " I 1 4 I | ' • " | I , . . | I , I . | , . , ! | . "' I 1'11" " I "1 0 "5 " Tl/Z--> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1032 2-Chloroethanol 3h 340 3 60 3.80 4 00 4.20 m/z 85.10 7.62%

5000-

n/z-> ■ 0- 12118 TTTTTTTHHH 0 5 24 113538 15. 27 43 49 53 586164 . | 11 11111 111 f-rrt^ 1 f. । ,, 1111 76 80 11 1 1 1 11 1111111 111; 11 ’T’ 111,111 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m y 3.40 3 60 3 80 4 00 4.20

08067.D 041202SCAN.M Tue Apr 16 13:56:07 2002 Page 5

NYC-WTC_000046807

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NYC-WTC_000046807Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE07978, Apr 2002 · Box DEP Box 27

NYC-WTC_000046707

Laboratory report documenting the GCMS analysis of sample AE07978 including surrogate recovery data and unknown compound screening on April 18, 2002.

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