GCMS analysis results, sample AE12478, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052902\12478.D Vial: 20 Acq On : 30 May 2002 1:34 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Acetic acid, chloro-, ethyl... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 3.98 0.65 ug/L 459312 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, chloro-, ethyl ester 122 C4H7C1O2 000105-39-5 2 Ethyl Chloride 64 C2H5C1 000075-00-3 4 3 2-Chloroethanol 80 C2H5C1O 000107-07/ 2 4 1-Propanol, 3-chloro- 94 C3H7C10 000627-3 -5 2 Abundance Scan 152 (3.972 min): 12478.D (-149) (-) m/z .49.10 100.00% 49

5000

35 1 56 82 3.60 3.80' ‘ 4.00 “ 4.20 ' 4.40 m/z-> of *m I 43 10 20 30 40 50 60 70 80 90 100 110 120 130 m/z 51.10 _/ 25.56% Abundance #108005: Acetic acid, chloro-, ethyl ester 29

5000 * i * 1 ’ * I * * • * i * * * ‘ i * ‘ * ‘ i 1 77 3.60 3.80 4.00 4.20 4.40 42 49 m/z 81.90 13.61% 14

miz- > of - 10 20 ++35— 14+450 60 70 801 889094 100 107110 120122 130 30 40 59 65 ■‘I I"Fru ■ 1 1 I 111’* I'l l | I । I ... । I i ■ < । ■

Abundance #107943: Ethyl Chloride 23 (T/VAAAAAMAMAMAWMI 3.60 3.80 4.00 4.20 4.40 64 5000 m/ Z 58.10 13.46% 49 35 15 I j nr ■ ' 11, ■, 'T1' • 01 - ' i ■ • ■ • i • ■ • ' i ■ ■ ■ ■ i • 1 ■ • i1 ‘ ■ i ‘ ■ i ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #108293:2-Chloroethanol • ■ i ■ ■ TIf 31 3.60 3.80 4.00 4.20 4.40 ^m/^^ 5000

m/z—> 0 ■ * i ■ 10 ■ i • ■ ■ * i 1,37/11.49, 61 ■ i ‘ 80 • i ■ • • 'I 1 ■ ■ ■ i • • ■ ■ i ■ 1 (1 i1 ■ 1 • i • • ■ ' i 1 ' । • ■ ■ • । 1 ■ • ‘ । ■ 1 t' ■ i ■ 1 1 ■ । ■ ■ 20 30 40 50 60 70 80 90 100 110 120 130 3.60 3.80 4.00 4.20 4.40

12478.D 052202.M Mon Jun 03 11:40:32 2002 Page 10

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