GCMS analysis results for sample AE11932, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11932.D Vial: 12 Acq On : 23 May 2002 6:56 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 Acetic acid, chloro-, ethyl... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

3.85 0.76 ug/L 518187 1,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qua! 1 Acetic acid, chloro-, ethyl ester 122 C4H7C1O2 000105-39-5 2 2 Ethyl Chloride 64 C2H5C1 000075-00-3/2 3 Borane, trifluoro- 68 BF3 007637-07-2 1 4 1-Propanol, 3-chloro- 94 C3H7C10 000627-30/5 1 Abundance Scan 131 (3.849 min): 11932.D (-130) (-) m/z 49.10 0.00% 40

5000 41 35 " r ■ " • i ■ ■ ■ ■i ■ 1,11 ■ 83 3.60 3.80 4.00 4.20 0- . 1’ 1 । .... । i . m/z 41.05 25.00% n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance 29 #108005: Acetic acid, chloro-, ethyl ester 4"hM/as 5000 1 ■ ■ ■ i ■ ■ ■ ' i ■ ' ■ ‘ I ■ ■ ■ ■ i ■ ■ ■

77 3.60 3.80 4.00 4.20 42 49 m/z 37.10 23.54% 14

/z-> 0 mlll 0- 10 20 30 35 i, , । 59 65 | 88 94 107 ■■■ ■ 1 — ■ ■ i ■,'1 ■ i ■ ■ ■'' i ■ 1 • ■ i 11 ■ ■ i ■ 40 50 60 70 80 90 100 110 122 120 130 Aao"“WAWww Abundance #107943: Ethyl Chloride

■ ■ ■ • i ■ 1 1 • i ' ■ ■ 1 i ‘ 1 ■ ■ i • ■ ■ 3.60 3.80 4.00 4.20 64 m/z 44.15 21.14% 5000

niz-> 15 35 49

0- ■■i ■ I rl ■ i 11 I'' I, ■ ■ ’I’p’ ■ ■ 111 ■ i ‘ ‘ i ■ ■ ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ i ■ ■ ■' i' ■ ‘ ■ i • Abundance 0 10 20 30 40 50 60 70 80 90 100 110 120 130 #12321: Borane, trifluoro- 1 1 1 ‘ I ‘ ' YWVr I ‘ ' 40 3.60 3.80 4.00 4.20 m/z 39.20 20.74%

5000 A

68 o- . .11 .19 .30 38 . , -10 18.8 /z-> o 10 20 30 40 50 60 70 80 90 100 110 120 130 3.60 3.80 4.00 4.20

11932.D 052202.M Wed May 29 09:51:36 2002 Page 9

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