GCMS analysis results, sample AE12478, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052902\12478.D Vial: 20 Acq On : 30 May 2002 1:34 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L ********************************************************************* Peak Number 6 Dicyandiamide Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 3.93 0.85 ug/L 600153 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Dicyandiamide 84 C2H4N4 000461-58-5 4 2 Thiophene 84 C4H4S 000110-02-1 4 3 Thiophene 84 C4H4S 000110-02-1 4 4 Azetidine, 1-nitroso- 86 C3H6N20 015216-10-1 4 Abundance Scan 144 (3.925 min): 12478.D (-142) (-) m/z 84.00 100.00% 84

5000 51

58 ■ ■ ■ i ■ ‘ • i • • • ■ i • ‘ ■ i ■ ■ ■ ■ । 37 41 3.60 3.80 4.00 4.20

iz-> Abundance 0- o mmmmmmMHT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #33614: Dicyandiamide “■i" Tamut Trr[Trrr|TT m/z 86.00 70.85%

84 43

5000 68 3.60 3.80 4.00 4.20 28 m/z 51.00 47.32% 22 | 32 39, , / 0- ... 1111»11 TTWTTTTT +PHT 53 58 npmpmpm tmppe miz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33732: Thiophene 84 ‘I 45 58 3.60 3.80 4.00 4.20 5000 m/z 49.10 40.00% 39

miz-> 0- 12 26 32 -I | 1 1 I 1 | 1 I t I | ! I I I | ! I I I | I I I I | I | I 1 | I I I I | I ! r 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 +52444..64..8Q,1l488,. TI’T Abundance #116584: Thiophene T 84 3.60 3.80 4.00 4.20 58 m/Z 58.00 20.12% 45 5000 39 50 69

n/z—> 0 m t+ 26 32 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Il I I | 1 I II 0 +mmlRHH7 TIT ‘II 3.60 TTI 3.80 4.00 4.20

12478.D 052202.M Mon Jun 03 11:40:32 2002 Page 9

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