GCMS analysis results for sample AE07978, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020415\07978.D Vial: 18 Acq On : 16 Apr 2002 12:44 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 2 Acetyl chloride Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

3.79 0.22 ug/L 188082 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetyl chloride 78 C2H3C10 000075-36-5 4 2 1-Propanesulfonyl chloride 142 C3H7C1O2S 010147-36-1 2 3 1-Tetrazol-2-ylethanone 112 C3H4N40 1000195-06-4 2 4 3-Acetoxy-2-trifluoromethylbuthe... 240 C9H11F3O4 1000222-26-4 2 Abundance Scan 122 (3 796 min): 07978 D (-119) (-) m/ z 43.30 100.00% 48

5000- 51 83 * , MMXs), AN, A A,/M 3.40 3 60 3 80 4.00 4.20 0- ■ ’ I ' ■ ■ ' I l 1 ■ ■ I ' 1 ' ' I ■ ■ ■ ’ I 1T m/z 51.20 25.12% n/z— > 0 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #3868 Acetyl chloride 43 MMAwMM*l,ya 15 5000 3.40 3.60 3.80 4.00 4.20 36 63 m/z 42.30 20.70% 28

n/z—> 0—T 0 — 121 2-ll, Ii I1 149.. 78......... 11'i■■■■i1■■■।''''।■ ■ ■ • ।' ।111 11111111 111 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #4066. 1-Propanesulfonyl chloride 43 —

3.40 360 3.80 4 00 4.20 5000- 27 m/z 83.10 19.19%

15 37 . 64 99 107 H4 n/z->0 4 0 r ,| rp” 4l,-pr 10 20 III, 1 30 1 1 40 +49584 50 60 70 76 83 80 90 i1 ■ 1 1 i ■ ■ ■ 1 i 1 1 1 1 .. .............. 1 1 1 1 i 1 100 110 120 Abundance #4641 1-Tetrazol-2-ylethanone ... .................... A 43 3.40 3.60 3 80 ' 4 00 ' 4 20 m/z 48.20 17.56% 5000

28 55 69 84 113 0 i ' 1 1 1 i r ■ ■ ■ । -PPP 1’1******/ I ■ ■ I Ouir l I I ' I > > I Tl/Z—> 0 10 20 30 40 50 60 70 80 90 100 110 120 3 40 3 60 3 80 4.00 4.20

07978.D 041202SCAN.M Tue Apr 16 13:47:46 2002 Page 5

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