GCMS results for sample AE08068, Apr 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08068.D Vial 25 Acq On : 16 Apr 2002 6:25 am Operator Nefliu Sample : sample Inst Instrumen Mise Multiplr 1.00 MS Integration Params: LSCINT.e Quant Method : C: \MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 18 Pentane, 2,4-dibromo- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

8.05 1.26 ug/L 830867 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentane, 2,4-dibromo- 228 C5H10Br2 019398-53-9 40 2 Pentane, 1,5-dibromo- 228 C5H10Br2 000111-24-0 40 3 Pentane, 1,4-dibromo- 228 C5H10Br2 000626-87-9 40 4 2-Butenoic acid, 4-nitrophenyl e... 207 C10H9NO4 014617-88-0 35 Abundance Scan 846 (8.050 min)' 08068.D (-839) (-) m/z 69.30 100.00% 69 55 41 91 5000 105 149

■n/z—> 0+ 20 40 li H 4 60 80 -- 100 120 . .... I.... ........ . 140 160 180 200 220 m/z 7 80 8 00 55.30 8.20 8.40 66.32% Abundance #136 Pentane. 2.4-dibromo- 23 41 69

5000 . _ ____________________ 7 80 8 00 8.20 8 40 m/z 41.25 56.25% 53 109 151 15 1 80 01 — Il UI‘ I 1 1 — I l ...... .......... . z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #114177: Pentane, 1,5-dibromo- 69 L 7 80 P OGnnn—nTT 8 00 8 20 8.40 5000 41 m/ z 91.30 51.26% 150 27 55 107

Tl/Z--> 0+ -5,4 20 40 —

60 81 80 93 100 || 121 135 120 140 160 180 200 220 230

Abundance #2438: Pentane, 1,4-dibromo- 41 69 7 80 8 00 8.20 8.40 m/z 39.30 34.89% 5000 27

T)/Z—> 0 15 53 | 11 | Jj 20 40 60 1 80,93107123 80 .....149I ....................... 100 120 140 160 180 200 220 _A 7 80 8.00 8.20 8.40

08068.D 041202SCAN.M Tue Apr 16 13:56:54 2002 Page 21

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