GCMS analysis results, Sample AE08267, April 22, 2002

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GCMS analysis report for sample AE08267 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048421–000048435

Folder label: “GCMS X 4/9/02 A 4/17/02”

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NYC 9/11 Public Portal Document

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Data File C:\MSDCHEM\1\DATA\020417\08267.D Vial: 24 Acq On 18 Apr 2002 4:22 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Phenanthrene-dlO Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.61 ug/L 1062580 Phenanthranene-dl0 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 87 2 Anthracene-dlO- 188 C14D10 001719-06-8 80 3 Pentacyclo[7.3.1.1. (4,12) . 0 (2,7) . . . 188 C14H20 1000215-61-8 45 4 5-Oxazolecarboxamide, 2-phenyl-188 C10H8N2O2 039819-42-6 38 Abundance Scan 3420 (23.174 min): 08267.D (-3414) (-) m/z 188.10 100.00% 188

5000

80 94 22.80 2300 23 20 23.40 23.60 43 57 66 .i 102 0-T hrijt th- ........ ......................... ............. m/z 189.10 16.15% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

.... ) 5000 TII+Iv........ 22 80 23.00 23 20 23.40 23 60 80 m/ z 80.05 13.58% 94 160 30 42 52 " n/z—> | 102110118 132 146 -170189—— 0 I ■ ■ " l ■' ' '11 ■' 'I" ।1111" I'1111" ''I " 111 11" 11" 11" 1111 "11111 ■ I■111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d ID- 188

22 80 23 00 23 20 23.40 23 60 5000 m/z94.10 12.97%

80 94 160 66

n/z- > 17 30 42 52 1 , 102 +..170.1894 Tur 118 01'■ 111" 111 '-n-i" ■ ।11 111111 |< 11.1■■11 —mmmtmtmutn 132 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 146

Abundance #79715: Pentacyclo[7 3 1 1 (4.12) 0(2.7) 0(6.11 )]tetradeca ■ l • ■ ' 1 I ' ^1 ' ' ■ ■ l .............. 188 22.80 23.00 23.20 23.40. 23.60 m/z 184.10 9.93%

5000 79 91 A 55 67 131 105 117 145 159

Tl/Z-> 9 I " " 11" '1111 'I' JU | Allol 1 j... I । I 111 > 1. 173 ।. 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 B’ur TII / 1 22.80 23.00 23.20 23.40 23.60

08267.D 041702SCAN.M Thu Apr 18 10:01:02 2002 Page 8

NYC-WTC_000048432

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