GCMS analysis results, Sample AE08265, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08265.D Vial: 22 Acq On : 18 Apr 2002 2:44 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 13 Benzenemethanol, 2,4,5-trim... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

35.02 0.20 ug/L 239351 Perylene-dl2 34.79

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Benzenemethanol, 2,4,5-trimethyl- 150 C1OH140 004393-05-9 9 2 2-Hydroxy-8-pyridin-2-yl-oct-7-e... 216 C13H16N2O 1000187-77-0 9 3 N-(2-Phenylethyl)-pyrrolidin-2 ,5... 203 C12H13NO2 1000145-69-9 9 4 Benzene, methyl(1-methylethenyl) - 132 C10H12 026444-18-8 5 Abundance Scan 5437 (35 025 min). 08265.D (-5435) (-) m/z 40.00 100.00% 43 132

5000 84 96 118

263 34 60 34.80 35.00 35.20 35 40 0 t-pT n m/z 132.20 78.91% ............... i ■ ' 1 1 i ' ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #59790: Benzenemethanol, 2,4,5-trimethyl- 13 2

150 91 107 5000 39 ' ■ i 1 1 ' i ' ■ 77 119 34.60 34 80 35.00 35.20 35.40 51 m/z 127.90 46.88% I I — h lh., .,Jl, M . 0 d" n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #59677: 2-Hydroxy-8-pyrldin-2-yl-oct-7-enenitrile 13 2

117 34.60 34.80 35.00 35.20 35.40 5000 m/z84.00 42.58% 93 161 106 27 39 51 65 78 n/z-> 0+ T* 4 ilL, r 1 l 20 40 60 80 —ll 100 120 140 160 172 189200 216 1. I- [ ‘ l .}

180 200 220 240 260 Abundance #52592: N-(2-Phenylethyl)-pyrrolidin-2,5-dione 1 7

145 m/z95.80 40.82% 90 5000 79 128

Tl/Z-> 62 I 0- ।1 r 11i1 1 * ■ । । । 1 i ■ ■ ■ । 20 40 60 80 ■ 100 120 102 1 1 f " I ' ■ | 1 ■ 1 ■ ( I 1 > 1 | 1 1 I I | 1 • 1 1 | ■1 > 1 1 | I — । । । i 140 160 180 200 220 240 260 1 lAAAAMAAAMh 34.60 34.80 35.00 35.20 35 40

08265.D 041702SCAN.M Thu Apr 18 09:58:19 2002 Page 18

NYC-WTC_000048399