GCMS analysis results for sample AE10813, May 2002

NYC 9/11 Public Portal Document

■ Data File : C:\MSDCHEM\1\DATA\051402\10813 .D Vial: 23 Acq On : 15 May 2002 8:17 am Operator: Mclean Sample : 5/7 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.52 ug/L 643422 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO 188 C14D10 001517-22-2 83 2 Anthracene-dlO- 188 C14D10 001719-06-8 72 3 4-Methyl-2-(3 - fluorophenyl)pyrim.. . 188 C11H9FN2 076128-66-0 40 4 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 40 Abundance Scan 3409 (23.109 min): 10813.D (-3402) (-) m/z 188.15 100.00% 188

5000

' ' i 1 1it I ' r’tb ‘d ‘ "I 80 94

m/z-> 42 hrrpapr h■.111h.. 111. ..... 0 . . ........... TTTT 57 66

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160170 180 190 ‘i B,U | 132 ......... Mt.. 22.80 23.00 23.20 23.40 m/z 189.20 15.63% Abundance #79827: Phenanthrene-d10 188

/ 5000 Tl I ’ll I J I I I > I I- I — I ’fB I- l— I

22.80 23.00 23.20 23.40 m/ z 94.00 14.19% 80 94 160 30 42 52 I J r66I !' I rrH I I I I I I I I 'I I I108 118 132 146 , |,I 170179/. 0 11 l" I l" I i I I I I I I I I I I I I I I I I r I I I i I I I I I J 1 I M'I !• I । I I I I 1'1 I I ri'lyri rrj'1 rrrftT

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 ‘ 1 I ' ' 1 ' I ' ' 1 1 I 1 1 ' 1 I ' 1 ' 1 I 22.80 23.00 23.20 23.40 5000 m/z 184.10 11.66%

RR 80 94 160 , | 17 30 42 52 ° I 108 118 132 146 ,i| 170179 . 0 TITT i | > i i r 1TTr ] t i r i "l i i [ I' I I i । i i I I J t r i tt1 ri FTFI । । । । । । । । | r I I । । I । I । । । I ri'I'i । । i [ > । < । | I'l'l m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79744:4-Methyl-2-(3-fluorophenyljpyrimidine 188 22.80 23.00 23.20 23.40 m/z 158.10 10.23%

5000 121

67 173 94 I 134 146 1 61 |, 39 50 .1. । 82 I, 108 ............... I............................. ri 111 n l’l I 1 I I ! ] 1 I 1 1 I > I > I I I ITTTi I [ > I I I lJT i i i | । ! I t [ r I I i । i i i । |" । r । । । ।11 । f [ i । Il....... 0 'T' " 11 ' 1 I ' ' 1 r1 . . /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10813.D 050102.M Thu May 16 14:15:52 2002 Page 10

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