GCMS analysis results for sample AE03250, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03250 conducted on March 15, 2002.

NYC-WTC_000006186–000006205

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03250.D Vial: 5 Acq On : 1 Mar 2002 7:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Thiocyanic acid, 2-benzothi... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 112548 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 59 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 3 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 4 1,5-Naphthalenedithiole 192 C10H8S2 000000-00-0 45 Abundance Scan 1675 (22.283 min): 03250.D (-) m/z 192.00 100.00% 1912

5000 —

49 70 — 82 96 ,1 120 146 160 22.00 22.20 22.40 22.60 0 1 ' 1 1 ''l " ' ' I " 1 1 irtrj ll l I | ! I I I | mrrri tt pomm TTTT m/z 191.00 18.08% mfe-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102098: Thiocyanic acid, 2-benzothiazolyl ester (CAS) $$ ... 192

5000 —.. -r... P 22.00 22.20 22.40 22.60 m/z 146.10 14.95% 6 82 90 108 122! 134| 148 160 A 0 1.......... ,U l'°' "I,.!....... I,. ■■ ——PPPPPT n/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 ....... A ' ' i 1 ' 1 ' i 1 '

m/z 4 22.00 22.20 22.40 22.60 96.00 14.84% 5000

96 165

m/z—> 88 J 139 152 176 0 i11'' r ■ ■1 r 1 ■ ■ r 11' r 1111 ■1'11' ■ ‘ ■ i ■ ■1 ‘ i11'11111 ‘'r ■1111 ■' ■ i 1 TTTT TH 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 192 22.00 22.20 22.40 22.60 m/z 193.00 14.37%

5000

144 177 0 0—00—00000000 —0011—20110001/00011010111001—1007* I'1 r ■ 1 1 1 ■ ■ 1 i > ■ < ■ । TTTT m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

)3250.D HP022102.M Mon Mar 04 12:33:42 2002 Page 14

NYC-WTC_000006203

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