GCMS analysis results for sample AE03250, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03250 conducted on March 15, 2002.

NYC-WTC_000006186–000006205

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document **LX**

Data File : C:\MSDCHEM\1\5973N\02MAR01\03250.D Vial: 5 . Acq On : 1 Mar 2002 7:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 1-Octadecanol (CAS) $$ Sten... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 26.18 0.09 ug/L 75424 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Octadecanol (CAS) $$ Stenol $$ . . . 270 C18H380 000112-92-5 64 2 1-Octadecanol (CAS) $$ Stenol $$... 270 C18H380 000112-92-5 59 3 Trifluoroacetic acid, n-tetradec... 310 C16H29F3O2 000000-00-0 53 4 1-Tridecene 182 C13H26 002437-56-1 50 Abundance Scan 2020 (26.178 min): 03250.D (-) m/z 55.10 100.00% 43 5? 83 97 69

5000 111 125 25.80 26.00 26.20 26.40 26.60 Ok/ IIT ■ ' 1 1 । 1 1 ■ ■ i 1 ' ■ ■ । ■ ■ ■ ■ । 1 ' 1 1 i 1 1 ' ' i 1 1 1 1 i 1 1 1 1 i 1 ■ 1 1 i m/z 57.10 97.02% ti/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #214167:1-Octadecanol (CAS) $$ Stenol $$ Sipol S $$ Stear... 43 55

5000 69 83 25.80 26.00 26.20 26.40 26.60 97 m/z 83.10 92.57%

m/z-> OmI tbif 1 1 I 40 60 80 —11125 100 111

120 224 252 T ' ■ | 1 > ' ' T-1-1 1 1 I ' 1 1 1 I ' 1 1 1 1 ■1 1 ' 1 Prt ' J 140 160 180 200 220 240 Abundance #214168:1-Octadecanol (CAS) $$ Stenol $$ Sipol S $$ Stear... 43 57 69 . ..... .0......... 25,80 26.00 26.20 26.40 26.60 5000 83 m/z 97.10 90.99% 97 111 O-TT i i 1 1 117 ------------------------- m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #260466: Trifluoroacetic acid, n-tetradecyl ester 43 25.80 26.00 26.20 26.40 26.60 55 m/ z 43.10 85.88% 69 5000 83 97 111 _

miz-> 0 ■ ■ i' ' 1 40 60 ll 100 ,| | 125 uo 1 ' 11 1 1 1 • ■ " । 80 168 । 196 । 1 1 ■ > | > ■ ■ ■ । 1 i ■ ■ । 120 140 160 180 200 220 240 ■ 1 । । ■ I ■ । > > I । । 1 > I 25.80 26.00 26.20 26.40 26.60

)3250 .D HP022102.M Mon Mar 04 12:33:42 2002 Page 15

NYC-WTC_000006204

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