GCMS analysis results for sample AE03252, March 2002

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Data File : C:\MSDCHEM\1\5973N\02MAR01\03252.D Vial: 7 Acq On : 1 Mar 2002 8:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Octadecane, 1-(ethenyloxy)-... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

28.49 0.06 ug/L 41462 Chrysene-dl 2 30.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Octadecane, 1-(ethenyloxy)- $$ E... 296 C20H40O 000930-02-9 59 2 Borane, diethylmethyl- (CAS) $$ ... 84 C5H13B 001115-07-7 43 3 1-Octadecanol (CAS) $$ Stenol $$... 270 C18H380 000112-92-5 40 4 l-Tridecanol (CAS) $$ n-Tridecan... 200 C13H280 000112-70-9 38 Abundance Scan 2225 (28.492 min): 03252. D (-) m/z 55.00 100.00% 55 ft 5000 4 69 83 97 111 . ....... M.... 28.20 28.40 28.60 28.80 OT ‘ ■ ।1 m/z 57.10 81.38% m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #245662: Octadecane, 1-(ethenyloxy)- $$ Ether, octadecyl v... 43 57

5000 83 28.20 28.40 28.60 28.80 27 70 m/z 43.10 56.04% , 97 O-TT i 111........................................ 278 296 z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #3398: Borane, diethylmethyl- (CAS) $$ Methyldiethylborane... 57 71 28.20 28.40 28.60 28.80 5000 m/ z 83.10 48.53% 5

O-TPTTT /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #214168:1-Octadecanol (CAS) $$ Stenol $$ Sipol S $$ Stear... 43 57 28.20 28.40 28.60 28.80 "z 69.10 44.98%

5000 70 83 97 111 0 1111111' TII TTT I....................... 1 ■ 'i1 ■1 ■ i ■1 > > । ■ ■ ■ ■ । ■' ■■।■■■■।■■ ■ ■ । ■11'11 > ।'' । > 111' 11' m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 28.20 28.40 28.60 28.80

'3252.D HP022102.M Mon Mar 04 12:33:55 2002 Page 14

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