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GCMS analysis results for sample AE00841, Feb 26 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS scan results for sample AE00841, including detection of unknown compounds and surrogate recovery data.

NYC-WTC_000052311–000052329

Folder label: “GCMS X 1/11/02 A 2/7/02

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Scanned page image, NYC-WTC_000052319
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00841.D Vial: 4 Acq On : 7 Feb 2002 1:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L **************************************************************** * * *** Peak Number 3 Butane, 2-methoxy-2-methyl-... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.92 0.49 ug/L 209794 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 36 2 3-Pentanol, 2,4-dimethyl- 116 C7H16O 000600-36-2 33 3 3 -(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 4 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 Abundance Scan 223 (5.920 min): 00841 .D (-) m/z 73.10 100.00% 7t3

5000.

43 1 5.60 5.80 6.00 6.20 m/z-> Onuurp 20 30 mllR 80 90 100 110 120 130 140 150 160 170 180 40 50 60 70 87 103 1asesdap*atu21s111dsduddd/*uI/ ■ । ■ ■ ■ ■ ।' m/z 43.10 23.84% Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73

5000 55 87 _M m/z 5.60 5.80 45.10 6.00 6.20 9.78% 27 45 | 0 ' r '' ■ r ' " i " '' i ■ TTT +PP ’ ’’’’11 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17065: 3-Pentanol, 2,4-dimethyl- 73 5.60 5.80 6.00 6.20 5000 55 m/ z 71.10 8.33% 43 27 11..... 0- ■ r '' ■ i ■11111 .... ........... 83 Ti n/z-> 20 30 40 50 60 70 80" I " ‘' I' ’111'1 " I' " 'I'' " I 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3’-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 .... A,i.. 5.60 5.80 6.00 6.20 m/ z 41.10 8.24%

5000

43 27 55 |.... 87.......... 113............................... 174 \A... 0 1111 ।11" ‘11 ' i ■''' i'' ’11' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00841.D HP020702.M Thu Feb 21 09:58:01 2002 Page 5

NYC-WTC_000052319

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NYC-WTC_000052319Source: NYC Law Department, mirrored locally

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