GCMS analysis results for sample AE00110, Feb 2002

NYC 9/11 Public Portal Document Z

Data File : C:\MSDCHEM\1\5973N\02FEB04\00110.D vial: 4 . Acq On 4 Feb 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Butane, 2-methoxy-2-methyl-... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.88 2.79 ug/L 1479340 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 4 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 28 Abundance Scan 220 (5.885 min): 00110.D (-) m/z 73.10 100.00% 73

5000 43 ' ■ ■ ■ i ■ ‘ ■ i ■ ■ ■ ■ i ■ 1 • ■ i ■ ■ ■ ■

I I 55 . 87 103 5.60 5.80 6.00 6.20 0--Ppm api PBtgen i1 ■ ■ ■ i “ • ■ i i1 ■ ■ ■ i “ ■ • i T" m/z 43.10 24.97% niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73

5000 ■ ■ .TT fl fk . LI7"PPF I PT 5.60 5.80 6.00 6.20 55 87 m/z 45.10 9.77% 27t 45 0- ‘ I ’ ' ’ I ‘ ’ ‘ ‘ I *' “ 11,1 * I Tr‘ Ir ' ■ • i ■ ■ ■' i1'" i ■" ■ । " i “ ■11"'111 • ■ ■ i ■ “ ■ i" " i ‘ " i ■

iz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 34[1,3]dioxolan-2-ylpropyl ester 73 1 ' I 1T 5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.27% 43 27 55 87 113 0--TI4 11 ‘ ‘ “ i"1 ■ i1‘ -i “ ' ■ i' “ ‘ i ‘' i1 ■" i ■ “ ' i “ ■ ■ i ■ ‘ “ i " “ i174 ■1 “ i ‘ miz-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 5.60 5.80 6.00 6.20′1 m/z 71.10 6.33% 5000 43 27 55 , 87 113 174 miz—> 0- — ' I i ‘‘ , । 1′1′0111000110022102′1022200000 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 N 5.60 15.80 6.00 6.20

)0110.D SCAN508.M Tue Feb 05 09:47:01 2002 Page 8

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