Laboratory record documenting GCMS surrogate recovery data for sample AE00317 analyzed on January 10, 2002.
NYC-WTC_000050977–000050993Folder label: “GCMS X 1/7/02 A 1/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Data File : C:\MSDCHEM\1\5973N\02JAN10\00317.D Vial: 4 Acq On : 10 Jan 2002 10:57 am Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 5 Butane, 2-methoxy-2-methyl-... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.88 ug/L 1623690 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 36 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 Acetic acid, 3-(1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 Abundance Scan 220 (5.885 min): 00317.D (-) m/z 73.10 100.00% 73
5000
43
87 103 5.60 5.80 6 00 6.20
n/z-> . 0 11'1'111 55,... 1 ।" 11 Tr ■ ■ ■ i' ■'' i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ‘ ■ i1' ■ ■ i''' ■ i' ■' ■ i m/z 43.10 23.94%
Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73 ..ri । । 27. M) r „ , 5000 5.60 5.80 6.00 6.20 55 87 m/z 41.10 9.20%
m/z-> 27 0-TPPugr 45
20 30 40i 50 XIu PTT TT 60 70 80 90 100 110 120 130 140 150 160 170 180 I i ■' • • i ■ i' ■'' i ■ ■' ’ i ■ ■' ■ i I'11 11
Abundance #36138: 3-(CYCLOHEX-3‘-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 ---------------------- 5.60 5.80 6.00 6.20 5000 m/ z 45.10 9.08% 43 27 55 87 113 174 0--TTTTt 11" ■11" ' • i • Biij 1 II’Ittr"bdsudw*su""B*I’**SI*’’I* /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester —12 7t3 5.60 5.80 6.00 6.20 m/Z 71.10 6.74%
5000 43 27 55 87 113 174 0 ■ r •1 ■ i ■1 TTTr Mr l ■ ■ i ■ r "'I1'" i' ■ ■ • i ■ ■ • ■ । 111111 T’ 1' ' I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 560 5.80 6.00 6.20
)0317.D SCAN508.M Thu Jan 10 11:52:17 2002 Page 7
NYC-WTC_000050988
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000050838
Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050963
Laboratory record documenting GCMS surrogate recovery data for sample AE00316 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050875
Laboratory record documenting GCMS surrogate recovery data for sample AE00279 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050912
Laboratory record documenting GCMS surrogate recovery data for sample AE00281 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051755
GCMS analysis log for sample AE00561 showing surrogate recovery and unknown compounds detected on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051685
Laboratory report showing GCMS analysis results for sample AE00365 conducted on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051768
GCMS analysis log for sample AE00557 showing surrogate recovery and unknown compounds detected on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050932
Laboratory record documenting GCMS surrogate recovery data for sample AE00282 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050856
Laboratory record documenting GCMS surrogate recovery data for sample AE00278 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051740
GCMS analysis log for sample AE00560 showing surrogate recovery and unknown compounds detected on January 17, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000050813
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050814
Fragmented page from a DEP laboratory record showing method parameters and sample data fields for January 7-9, 2002 testing.
Filed in the same folder
NYC-WTC_000050817
Technical form detailing GCMS analysis results for sample AE00277 listing detected compounds and concentrations from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050821
Reference report for GCMS analysis of sample AE00277 listing compound names and qualifier values from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050825
Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.
Filed in the same folder