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GCMS surrogate recovery results for sample AE00277, Jan 2002

Machine-extracted title · confidence 90%

Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.

NYC-WTC_000050838–000050855

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050850
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\5973N\02JAN09\277.D Vial: 2 Acq On 9 Jan 2002 6:59 pm Operator: Sample 508 scan ext 1/7 Inst : Instrumen Mise January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ************************************************************* * * * * * * * * Peak Number 6 3-(CYCLOHEX-3'-EN-YL)PROPAN. .. Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.38 ug/L 1925250 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 33 4 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 33 Abundance Scan 220 (5.885 min): 277. D (-) m/ z 73.10 100.00% 73

_ y n" I ■ r . . 5000 43 87 103 5.60 5.80 6.00 6.20 ............................. ... Oh | ' >lF . 1 ' ' I '" ... ........ 1 1 1 1 ' I1 ।1111 • ■ ■ i • ■'' i ■l i■ ’ i i ‘' ' i1 ‘1 ■ i' m/z 43.10 25.15% n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance i#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 7(3

5000 5.60 5.80 6.00 6.20 43 m/z 45.10 9.82% 27 !55 । 87 113 174 0 -PPT +TTT r T’T’II’F’TITTTTS i >1 ■ ■ I < > ■ ■ । I' ''' I nlz-> 20 30 40 50• 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[ 1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.80% 43 27 87 113 0- TTT 11 "55■ ■ i •' ■ ■ i' i'' " i' " 11 174 ■I' 1 ' 1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17065: 3-Pentanol, 2,4-dimethyl- ‘ , rf । , 1 । . rr 73 5.60 5.80 6.00 6.20 m/z 71.10 6.55% 5000 55

43 27

n/z—> oV TL TTT1 4 TT‘ +83 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 r ''' I'''' i ■ ■'' i'''' i i1 ■ ’' I 5.60 5.80 6.00 6.20

:77 .D SCAN508.M Thu Jan 10 11:51:37 2002 Page 8

NYC-WTC_000050850

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NYC-WTC_000050850Source: NYC Law Department, mirrored locally

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