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GCMS analysis results for sample AE03252, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03252 conducted on March 15, 2002.

NYC-WTC_000006226–000006245

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006242
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NYC 9/11 Public Portal Document uDLaly sedcI Lopourd Keporc

Data File: C:\MSDCHEM\1\5973N\02MAR01\03252.D Vial: 7 • Acq On : 1 Mar 2002 8:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 1-Octadecanol (CAS) $$ Sten... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 26.18 0.04 ug/L 33218 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 1-Octadecanol (CAS) $$ Stenol $$... 270 C18H380 000112-92-5 50 2 Silane, trichloroeicosyl- $$ Eic... 414 C20H41C13Si 018733-57-8 40 3 1-Heptadecanol (CAS) $$ n-Heptad... 256 C17H360 001454-85-9 37 4 1-Heptanol, 6-methyl- $$ 6-Methy... 130 C8H18O 001653-40-3 22 Abundance Scan 2020 (26.178 min): 03252.D (-) m/ z 55.10 100.00% 55 83 43 97 69 5000 111 111 ’ I’’ 4 25.80 26.00 26.20 26.40 26.60 0 1 1 ' 1 ' 'T1 1 ' ' I 11 । 1 | ' • i ' ' m/ Z 83.00 94.20% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #214168: 1-Octadecanol (CAS) $$ Stenol $$ Sipol S $$ Stear... 43 57 69

5000 83 1 i ' 1 ■ ■ i ■ ■ I ' 1 । 1 । । ' 1 1 । 1 25.80 26.00 26.20 26.40 26.60 97 m/z 57.10 83.85% 111 0- 1 i ' ■ ■ ■ i ■ 1 ' ■ i 1 ' ■ ■ i ■ 1 ■ i ' ■ ■ I r1 1 1 1 1 ----- m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #339598: Silane, trichloroeicosyl- $$ Eicosyltrichlorosilane 41 55 ----- ■ l ■ - ■ ■ i ■ 25.80 26.00 26.20 26.40 26.60 5000 m/z 97.10 75.34% 69 83 97

mfe-> 27 0 ' i ' ■ ' 1 i ' ' ' ' i 20 30 40 ■ ■ i 1 50 ■ i ■ ' 60 70I 80 1n III, ' I ' ll ' ' 90 100 111 1 । P । । 1 । ii'1 । । । ! 110 120 130 125

Abundance #195647:1-Heptadecanol (CAS) $$ n-Heptadecanol $$ Heptade... 43 69 83 25,80 26.00 26.20 26.40 26.60 57 97 m/z 43.10 70.79% A 5000

. ................ ............................... , 01' i 1 1 1 1 r1 1 1 1 i 1 1 r 1 i ' 1 ■ ' i ' ' ■ ■ i 1 ■ ■ 1 । ■ ■ ■ 1 । 1 ■ ■ ■ । 1 ■ ■ 1 । ' ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 25.80 26.00 26.20 26.40 26.60

i3252. D HP022102.M Mon Mar 04 12:33:55 2002 Page 13

NYC-WTC_000006242

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NYC-WTC_000006242Source: NYC Law Department, mirrored locally

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