GCMS analysis results for sample AE02720, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02720 including surrogate recovery.

NYC-WTC_000011027–000011045

Folder label: “GCMS X 2/5/02 A 2/28/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report : C:\MSDCHEM\l\5973N\02FEB28\02720.D •. Data "File Vial: 5 Acq On : 28 Feb 2002 6:00 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 1-Heptadecanol $$ n-Heptade... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 26.18 0.75 ug/L 541745 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Heptadecanol $$ n-Heptadecanol... 256 C17H360 001454-85-9 94 2 Phosphonic acid, dioctadecyl est... 587 C36H75O3P 019047-85-9 93 3 1-Octadecanol (CAS) $$ Stenol $$... 270 C18H380 000112-92-5 90 4 1-Hexadecanol 242 C16H340 036653-82-4 87 Abundance Scan 2020 (26.177 min): 02720.D (-) m/z 55.10 100.00% 43 55 69 83 97 __

5000 111 125 ‘ I ’ ' • • I ’ ‘ ' • i ' ‘ ‘ ’ Tr184 I ‘ 25.80 26.00 26.20 26.40 26.60 m/z-> 0- TP 40 4 11 101.0140...... ........ 60 80 100 120 140 160 180 200 220 240 m/z 83.10 97.23% Abundance #195644:1-Heptadecanol $$ n-Heptadecanol $$ Heptadecyl al... 55 69 22 83 97 5000 111 25.80 26.00 26.20 26.40 26.60 125 m/z 57.10 94.01% 210 238 0p t/T ■ ' i 1 l • • * • ! • » • • । » • • • । । i ‘ । ’ I ‘ ‘ ’ f * ' ’ ‘ l * ‘ 1 ‘ 1 miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #380758: Phosphonic acid, dioctadecyl ester $$ Di(n-octade... 55 69 83 43 97 . . .0 25.80 26.00 26.20 26.40 26.60 5000 m/z 43.10 83.77% 111 ,1 125136 O-T ′ ■ I i 1 ■ ‘ ■ i ■ ■ ' ‘ i ' ■ ■ • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ • ■ 1 i miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #214166:1-Octadecanol (CAS) $$ Stenol $$ Sipol S $$ Stear... 1 | । 1 I m-1 । i i i i । i i inmn 43 55 69 83 25 80 26.00 26.20 26.40 26.60 97 m/z 97.10 83.15%

5000 111 i 125

n/z—> OTT ’rT ■ • ।1 40 60 80 Iaa.,9 100 ........... ......... 721.111252, 120 140 160 180 200 220 240 -Pmpp 25.80 26.00 26.20 26.40 26.60

02720.D HP022102.M Fri Mar 01 10:07:43 2002 Page 13

NYC-WTC_000011043

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NYC-WTC_000011043Source: NYC Law Department, mirrored locally

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