GCMS analysis results for sample AE02713, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.

NYC-WTC_000010867–000010886

Folder label: “GCMS X 2/5/02 A 2/28/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB28\02713.D Vial: 3 Acq On : 28 Feb 2002 12:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 12 Cyclohexane, 1,2,3-trimethy... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 26.18 0.07 ug/L 44003 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane, 1,2,3-trimethyl-, (... 126 C9H18 001678-81-5 50 2 1-Octadecanol (CAS $$ Stenol $$... 270 C18H380 000112-92-5 43 3 7-Oxabicyclo[4.1.0]heptane $$ Cy... 98 C6H10O 000286-20-4 38 4 Dodecanal (CAS) $$ n-Dodecanal 184 C12H240 000112-54-9 35 Abundance Scan 2020 (26.177 min): 02713.D (-) m/z 83.10 100.00% 43 55 83 97 69 5000 111

25.80 26.00 26.20 26.40 26.60 0 i■■■•। “ i i1' ■ ■ i1 ■ T’2’111011 -rrp-rrrp- ' " I " '‘ I 1 11 ' ' ‘ I “ " I 1’11117111 m/z 43.10 82.23% /z—> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 Abundance #23240: Cyclohexane, 1,2,3-trimethyl-, (1.alpha.,2.beta.,3... 41 55 69

5000 83 25.80 26.00 26.20 26.40 26.60 m/z55.10 77.96% 97

n/z—> 0- I ‘' I" " I • “' I' 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 115120 ....all.. ■। । ■'' • ।। •1 ■ ■ । । ।■

Abundance #214168:1-Octadecanol (CAS) $$ Stenol $$ Sipol S $$ Stear... 43 57 69 25.80 26.00 26.20 26 40 26.60 5000 83 m/z 57.10 76.79% 97 111 0 i‘ “i i “ • i ■ ■ “ i ■ ■' ■ np W—upr ■" ‘ i “ " i MAYaaapOans-Baspunnap /z—> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 Abundance #7216:7-Oxabicyclo[4.1 O]heptane $$ Cyclohexane, 1,2-epox... 41 83 25.80 26.00 26.20 26.40 26.60 m/z97.10 68.96% 55 5000 70 98

n/z—> 0 i‘" ‘ i1 ■ “ lp 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 ! t«• >»I •'1 * I • ' i ■1 ■ ■ i ■ • ■ ■ i ■ ■ ■ • i •' ■ ■ i ■ 25.80 26.00 26.20 26.40 26.60

02713.D HP022102.M Fri Mar 01 10:06:54 2002 Page 14

NYC-WTC_000010884

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GCMS analysis results, sample AE02719, March 2002 · Box DEP Box 14

NYC-WTC_000010987

Gas chromatography-mass spectrometry analysis of sample AE02719 performed March 5, 2002, reporting other unknown compounds and surrogate 2,4-DDD recovery data.

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