DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB01\31134.D Vial: 3 Acq On : 1 Feb 2002 4:24 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1’, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 9 Cyclohexasiloxane, dodecame... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 15.62 0.14 ug/L 93342 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 91 2 Cyclohexasiloxane, dodecamethyl-... 444 C12H3606Si6 000540-97-6 80 3 Acetic acid, bis[(trimethylsily... 356 C11H29O5PS13 053044-27-2 37 4 Acetic acid, bis[(trimethylsily... 356 CllH29O5PSi3 053044-27-2 37 Abundance Scan 1073 (15.624 min): 31134.D (-) m/ z 73.10 100.00% 73

341 5000 429 147

01- 45 Tuum 207 i" " i1'" i" " i" " i " “ r "' i" " r "' i" " i .......... 1 I II 1 1,1171 > I I I I I I I I I I I > I > I I I I I I I I 15.20 15.40 15.60 15.80 16.00 m/z 341.00 53.63% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #352522: Cyclohexasiloxane, dodecamethyl- 73

...................... ) 5000 341 15.20 15.40 15.60 15.80 16.00 429 m/z 429.10 27.59% 147

01.... urpuunm | 207 i11"i"" i■ ‘" i" ■' i " "i"“ i"" i' i 271 311, 1............. 11" 1111 ‘1111'' I"''I'1111'''11 mlz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #352523: Cyclohexasiloxane, dodecamethyl- $$ Dodecamethylc... 73 341 i ' 1 ' ■ i ■ ■ 15.20 15.40 15.60 15.80 16.00 429 m/z 147.00 5000 19.92%

147

n/z-> ol....1.. .. It.,,!,. ,.. I 207 267 111111111111111111111111111011011 40 60 80 100120140160180200220240260280300320340360380400420 311 L —1101137171 hmmmTTT Abundance #302661: Acetic acid, [bis[(trimethylsilyl)oxy]phosphinyl].„ 73 341 15.20 15.40 15.60 15.80 16.00 m/ z 32 5.00 15.51%

5000 251 133 299 211

Or ■ ।>■ ■ ■ i ■ • • ‘ i" ■•I *b" i ■ ■ > ■ i ■"'i■"' i' ■ - 1________________ "I" "I "l'll l 1 ■ ■ ■ i ' ■ 1 1 I 1 1 ' 1 I 1 1 m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 15.20 15,40 15.60 15.80 16.00

31134.D SCAN508.M Mon Feb 04 08:41:37 2002 Page 11

NYC-WTC_000004085

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999